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ethyl α(E)-[(diethylamino)methylene]-2,4,5-trifluoro-3-methoxy-β-oxo-benzenepropanoate

Base Information Edit
  • Chemical Name:ethyl α(E)-[(diethylamino)methylene]-2,4,5-trifluoro-3-methoxy-β-oxo-benzenepropanoate
  • CAS No.:925457-02-9
  • Molecular Formula:C17H20F3NO4
  • Molecular Weight:359.345
  • Hs Code.:
  • Mol file:925457-02-9.mol
ethyl α(E)-[(diethylamino)methylene]-2,4,5-trifluoro-3-methoxy-β-oxo-benzenepropanoate

Synonyms:ethyl α(E)-[(diethylamino)methylene]-2,4,5-trifluoro-3-methoxy-β-oxo-benzenepropanoate

Suppliers and Price of ethyl α(E)-[(diethylamino)methylene]-2,4,5-trifluoro-3-methoxy-β-oxo-benzenepropanoate
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The product has achieved commercial mass production*data from LookChem market partment
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Chemical Property of ethyl α(E)-[(diethylamino)methylene]-2,4,5-trifluoro-3-methoxy-β-oxo-benzenepropanoate Edit
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Technology Process of ethyl α(E)-[(diethylamino)methylene]-2,4,5-trifluoro-3-methoxy-β-oxo-benzenepropanoate

There total 2 articles about ethyl α(E)-[(diethylamino)methylene]-2,4,5-trifluoro-3-methoxy-β-oxo-benzenepropanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
Multi-step reaction with 2 steps
1: oxalyl chloride; DMF / CH2Cl2 / 24 h / 20 °C
2: 1.88 g / Et3N / toluene / 5 h / 90 °C
With oxalyl dichloride; triethylamine; N,N-dimethyl-formamide; In dichloromethane; toluene;
DOI:10.1016/j.ejmech.2006.07.003
Guidance literature:
Multi-step reaction with 2 steps
1: ethanol; diethyl ether / 3 h / 20 °C
2: 627 mg / K2CO3 / dimethylformamide / 5 h / 100 °C
With potassium carbonate; In diethyl ether; ethanol; N,N-dimethyl-formamide;
DOI:10.1016/j.ejmech.2006.07.003
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