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1-bromo-3,5-bis(octyloxy)phenyl

Base Information Edit
  • Chemical Name:1-bromo-3,5-bis(octyloxy)phenyl
  • CAS No.:937390-20-0
  • Molecular Formula:C22H37BrO2
  • Molecular Weight:413.439
  • Hs Code.:
  • Mol file:937390-20-0.mol
1-bromo-3,5-bis(octyloxy)phenyl

Synonyms:1-bromo-3,5-bis(octyloxy)phenyl

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Chemical Property of 1-bromo-3,5-bis(octyloxy)phenyl Edit
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Technology Process of 1-bromo-3,5-bis(octyloxy)phenyl

There total 7 articles about 1-bromo-3,5-bis(octyloxy)phenyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
5-bromoresorcinol; With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 0.5h;
1-bromo-octane; In N,N-dimethyl-formamide; at 60 ℃;
DOI:10.1039/c4ra10154e
Guidance literature:
Multi-step reaction with 2 steps
1: 43 percent / BBr3
2: K2CO3; Adogen 464 / acetone / Heating
With adogen 464; boron tribromide; potassium carbonate; In acetone;
DOI:10.1039/b615545f
Guidance literature:
Multi-step reaction with 4 steps
1: 96 percent / K2CO3; Adogen 464 / acetone / Heating
2: 86 percent / NaOH / methanol / Heating
3: SOCl2 / 2 h / Heating
4: 0.70 g / CBrCl3; 2-mercaptopyridine N-oxide sodium salt; AIBN / 1 h / Heating
With sodium hydroxide; thionyl chloride; adogen 464; 2,2'-azobis(isobutyronitrile); Bromotrichloromethane; 2-mercaptopyridine-1-oxide sodium salt; potassium carbonate; In methanol; acetone; 4: Barton decarboxylation;
DOI:10.1039/b615545f
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