C₅₈H₄₂

Base Information

• Chemical Name: C₅₈H₄₂
• CAS No.: 1062555-78-5
• Molecular Formula: C₅₈H₄₂
• Molecular Weight: 738.971
• Mol file: 1062555-78-5.mol

Synonyms:C₅₈H₄₂

Chemical Property of C₅₈H₄₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₅₈H₄₂

There total 5 articles about C₅₈H₄₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

anthracene-9-boronic acid (100622-34-2) → C58H42 (1062555-78-5)

Guidance literature:

Multi-step reaction with 3 steps

1: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene; ethanol; water / 24 h / 120 °C

2: N-Bromosuccinimide / dichloromethane / 24 h / 25 °C / Inert atmosphere

3: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene; ethanol; water / 4 h / 120 °C

With N-Bromosuccinimide; sodium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In ethanol; dichloromethane; water; toluene;

Reference yield:

9-Bromoanthracene (1564-64-3) → C58H42 (1062555-78-5)

Guidance literature:

Multi-step reaction with 4 steps

1.1: n-butyllithium / hexane; tetrahydrofuran / -78 °C / Inert atmosphere

1.2: 20 °C

2.1: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene; ethanol; water / 24 h / 120 °C

3.1: N-Bromosuccinimide / dichloromethane / 24 h / 25 °C / Inert atmosphere

4.1: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene; ethanol; water / 4 h / 120 °C

With N-Bromosuccinimide; n-butyllithium; sodium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; ethanol; hexane; dichloromethane; water; toluene;

Reference yield:

2,8‐dibromo‐6,6,12,12‐tetramethylindeno[1,2‐b]fluorene (872705-64-1) → C58H42 (1062555-78-5)

Guidance literature:

Multi-step reaction with 3 steps

1: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene; ethanol; water / 24 h / 120 °C

2: N-Bromosuccinimide / dichloromethane / 24 h / 25 °C / Inert atmosphere

3: sodium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / toluene; ethanol; water / 4 h / 120 °C

With N-Bromosuccinimide; sodium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In ethanol; dichloromethane; water; toluene;

upstream raw materials:

anthracene-9-boronic acid

9-Bromoanthracene

2,8‐dibromo‐6,6,12,12‐tetramethylindeno[1,2‐b]fluorene

6,6,12,12-tetramethyl-6,12-dihydroindeno[1,2-b]fluorene

Downstream raw materials:

C₅₈H₄₁Br

C₇₃H₅₄

Refernces