Technology Process of C58H44N2O2
There total 3 articles about C58H44N2O2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
tri-tert-butyl phosphine; sodium t-butanolate;
palladium diacetate;
In
toluene;
at 85 ℃;
for 7h;
Inert atmosphere;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: n-butyllithium / hexane; tetrahydrofuran / 3 h / -65 - 20 °C / Inert atmosphere; Heating
1.2: 3 h / -65 - 20 °C / Heating
2.1: sodium t-butanolate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl / tris-(dibenzylideneacetone)dipalladium(0) / toluene / 6 h / 85 °C / Inert atmosphere
3.1: sodium t-butanolate; tri-tert-butyl phosphine / palladium diacetate / toluene / 7 h / 85 °C / Inert atmosphere
With
n-butyllithium; tri-tert-butyl phosphine; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; sodium t-butanolate;
tris-(dibenzylideneacetone)dipalladium(0); palladium diacetate;
In
tetrahydrofuran; hexane; toluene;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: sodium t-butanolate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl / tris-(dibenzylideneacetone)dipalladium(0) / toluene / 6 h / 85 °C / Inert atmosphere
2: sodium t-butanolate; tri-tert-butyl phosphine / palladium diacetate / toluene / 7 h / 85 °C / Inert atmosphere
With
tri-tert-butyl phosphine; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; sodium t-butanolate;
tris-(dibenzylideneacetone)dipalladium(0); palladium diacetate;
In
toluene;
