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(S)-5-tert-butyl 6-methyl 5-azaspiro[2.4]heptane-5,6-dicarboxylate

Base Information Edit
  • Chemical Name:(S)-5-tert-butyl 6-methyl 5-azaspiro[2.4]heptane-5,6-dicarboxylate
  • CAS No.:1129634-43-0
  • Molecular Formula:C13H21NO4
  • Molecular Weight:255.314
  • Hs Code.:2933990090
  • Mol file:1129634-43-0.mol
(S)-5-tert-butyl 6-methyl 5-azaspiro[2.4]heptane-5,6-dicarboxylate

Synonyms:(S)-5-tert-butyl 6-methyl 5-azaspiro[2.4]heptane-5,6-dicarboxylate

Suppliers and Price of (S)-5-tert-butyl 6-methyl 5-azaspiro[2.4]heptane-5,6-dicarboxylate
Supply Marketing:Edit
Business phase:
The product has achieved commercial mass production*data from LookChem market partment
Manufacturers and distributors:
  • Manufacture/Brand
  • Chemicals and raw materials
  • Packaging
  • price
  • TRC
  • (S)-5-Boc-5-azaspiro[2.4]heptane-6-carboxylicAcidMethylEster
  • 50mg
  • $ 220.00
  • Crysdot
  • (S)-5-tert-Butyl6-methyl5-azaspiro[2.4]heptane-5,6-dicarboxylate 95+%
  • 1g
  • $ 752.00
  • Chemenu
  • (S)-5-tert-Butyl6-methyl5-azaspiro[2.4]heptane-5,6-dicarboxylate 95%
  • 1g
  • $ 711.00
  • Alichem
  • (S)-5-tert-Butyl6-methyl5-azaspiro[2.4]heptane-5,6-dicarboxylate
  • 1g
  • $ 740.52
Total 8 raw suppliers
Chemical Property of (S)-5-tert-butyl 6-methyl 5-azaspiro[2.4]heptane-5,6-dicarboxylate Edit
Chemical Property:
  • Boiling Point:328.9±35.0 °C(Predicted) 
  • PKA:-2.75±0.40(Predicted) 
  • PSA:55.84000 
  • Density:1.15±0.1 g/cm3(Predicted) 
  • LogP:1.88690 
Purity/Quality:

97% *data from raw suppliers

(S)-5-Boc-5-azaspiro[2.4]heptane-6-carboxylicAcidMethylEster *data from reagent suppliers

Safty Information:
  • Pictogram(s):  
  • Hazard Codes: 
MSDS Files:

SDS file from LookChem

Useful:
Technology Process of (S)-5-tert-butyl 6-methyl 5-azaspiro[2.4]heptane-5,6-dicarboxylate

There total 3 articles about (S)-5-tert-butyl 6-methyl 5-azaspiro[2.4]heptane-5,6-dicarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
Multi-step reaction with 4 steps
1.1: triethylamine
2.1: sodium periodate; ruthenium trichloride
4.1: diethylzinc; trifluoroacetic acid / hexane; dichloromethane / 1 h / -5 °C / Inert atmosphere
4.2: 72 h / -5 - 30 °C / Inert atmosphere
4.3: 24 h / 20 °C
With ruthenium trichloride; sodium periodate; diethylzinc; triethylamine; trifluoroacetic acid; In hexane; dichloromethane; 3.1: Wittig reaction / 4.1: Simmons-Smith reaction / 4.2: Simmons-Smith reaction;
DOI:10.1016/j.tetlet.2012.05.020
Guidance literature:
Multi-step reaction with 4 steps
1.1: triethylamine
2.1: sodium periodate; ruthenium trichloride
4.1: diethylzinc; trifluoroacetic acid / hexane; dichloromethane / 1 h / -5 °C / Inert atmosphere
4.2: 72 h / -5 - 30 °C / Inert atmosphere
With ruthenium trichloride; sodium periodate; diethylzinc; triethylamine; trifluoroacetic acid; In hexane; dichloromethane; 3.1: Wittig reaction / 4.1: Simmons-Smith reaction / 4.2: Simmons-Smith reaction;
DOI:10.1016/j.tetlet.2012.05.020
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