Welcome to LookChem.com Sign In|Join Free
  • or

Encyclopedia

4-BroMo-9,9-diphenyl-9H-fluorene

Base Information Edit
  • Chemical Name:4-BroMo-9,9-diphenyl-9H-fluorene
  • CAS No.:713125-22-5
  • Molecular Formula:C25H17Br
  • Molecular Weight:397.314
  • Hs Code.:2903999090
  • Mol file:713125-22-5.mol
4-BroMo-9,9-diphenyl-9H-fluorene

Synonyms:4-BroMo-9,9-diphenyl-9H-fluorene;4-BroMo-9,9-diphenyl-9H-fluorne

Suppliers and Price of 4-BroMo-9,9-diphenyl-9H-fluorene
Supply Marketing:Edit
Business phase:
The product has achieved commercial mass production*data from LookChem market partment
Manufacturers and distributors:
  • Manufacture/Brand
  • Chemicals and raw materials
  • Packaging
  • price
  • TRC
  • 4-Bromo-9,9-diphenyl-9H-fluorene
  • 100mg
  • $ 75.00
  • TCI Chemical
  • 4-Bromo-9,9-diphenylfluorene >98.0%(GC)
  • 5g
  • $ 329.00
  • TCI Chemical
  • 4-Bromo-9,9-diphenylfluorene >98.0%(GC)
  • 1g
  • $ 66.00
  • Crysdot
  • 4-Bromo-9,9-diphenyl-9H-fluorene 95+%
  • 10g
  • $ 141.00
  • Biosynth Carbosynth
  • 4-Bromo-9,9-diphenylfluorene
  • 2 g
  • $ 70.00
  • Biosynth Carbosynth
  • 4-Bromo-9,9-diphenylfluorene
  • 1 g
  • $ 45.50
  • Biosynth Carbosynth
  • 4-Bromo-9,9-diphenylfluorene
  • 10 g
  • $ 200.00
  • Biosynth Carbosynth
  • 4-Bromo-9,9-diphenylfluorene
  • 5 g
  • $ 135.00
  • Biosynth Carbosynth
  • 4-Bromo-9,9-diphenylfluorene
  • 25 g
  • $ 400.00
  • Arctom
  • 4-Bromo-9,9-diphenyl-9H-fluorene 97%
  • 25g
  • $ 284.00
Total 82 raw suppliers
Chemical Property of 4-BroMo-9,9-diphenyl-9H-fluorene Edit
Chemical Property:
  • Melting Point:213.5-214.5℃ (ethanol ) 
  • Boiling Point:480.5±24.0 °C(Predicted) 
  • PSA:0.00000 
  • Density:1.363±0.06 g/cm3(Predicted) 
  • LogP:6.81220 
  • Storage Temp.:Sealed in dry,Room Temperature 
Purity/Quality:

99.8% *data from raw suppliers

4-Bromo-9,9-diphenyl-9H-fluorene *data from reagent suppliers

Safty Information:
  • Pictogram(s):  
  • Hazard Codes: 
MSDS Files:

SDS file from LookChem

Useful:
Technology Process of 4-BroMo-9,9-diphenyl-9H-fluorene

There total 2 articles about 4-BroMo-9,9-diphenyl-9H-fluorene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
2,2'-dibromobiphenyl; With n-butyllithium; In tetrahydrofuran; hexane; at -78 - 70 ℃; for 2h;
benzophenone; In tetrahydrofuran; hexane; at -70 ℃;
Guidance literature:
With n-butyllithium; diethyl ether; at -20 ℃; anschliessend Behandeln mit Benzophenon;
DOI:10.1021/ja01591a053
Guidance literature:
Multi-step reaction with 2 steps
1.1: n-butyllithium / tetrahydrofuran / 1 h / -78 °C / Inert atmosphere
1.2: -78 - 20 °C
2.1: potassium carbonate; tetrakis(triphenylphosphine) palladium(0) / tetrahydrofuran; water / 5 h / Inert atmosphere; Reflux
With tetrakis(triphenylphosphine) palladium(0); n-butyllithium; potassium carbonate; In tetrahydrofuran; water; 2.1: |Suzuki Coupling;
upstream raw materials:

2,2'-dibromobiphenyl

benzophenone

Refernces Edit
Post RFQ for Price