Technology Process of 2-Methylamino-2-phenylbutanol
There total 7 articles about 2-Methylamino-2-phenylbutanol which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
lithium aluminium tetrahydride;
In
tetrahydrofuran;
for 8h;
Heating;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 99 percent / Ac2O / 15 h / 20 °C
2: 97.9 percent / LiAlH4 / tetrahydrofuran / 8 h / Heating
With
lithium aluminium tetrahydride; acetic anhydride;
In
tetrahydrofuran;
1: Formylation / 2: Reduction;
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 93 percent / MgSO4; Et3N / CH2Cl2 / 17 h / 20 °C
2: 85 percent / NaH; CuCl2 / tetrahydrofuran / 18 h / 20 °C
3: 99 percent / HCl; Et2O; H2O / 24 h / 20 °C
4: 95 percent / Et3N / tetrahydrofuran / 0.33 h
5: 99 percent / Ac2O / 15 h / 20 °C
6: 97.9 percent / LiAlH4 / tetrahydrofuran / 8 h / Heating
With
hydrogenchloride; lithium aluminium tetrahydride; diethyl ether; water; acetic anhydride; sodium hydride; magnesium sulfate; triethylamine; copper dichloride;
In
tetrahydrofuran; dichloromethane;
1: Condensation / 2: Alkylation / 3: Hydrolysis / 4: Dehydrochlorination / 5: Formylation / 6: Reduction;