N-cyclohexyl-N'-isopropylcarbodiimide

Base Information

• Chemical Name: N-cyclohexyl-N'-isopropylcarbodiimide
• CAS No.: 3496-83-1
• Molecular Formula: C10H18 N2
• Molecular Weight: 166.266
• Hs Code.: 2925290090
• Mol file: 3496-83-1.mol

Synonyms:Carbodiimide,cyclohexylisopropyl- (7CI,8CI); Cyclohexylisopropylcarbodiimide;N-Cyclohexyl-N'-isopropylcarbodiimide

Chemical Property of N-cyclohexyl-N'-isopropylcarbodiimide

Chemical Property:

• Boiling Point: 202.6°Cat760mmHg
• Flash Point: 67.8°C
• PSA: 24.72000
• Density: 0.96g/cm³
• LogP: 2.90140

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of N-cyclohexyl-N'-isopropylcarbodiimide

There total 7 articles about N-cyclohexyl-N'-isopropylcarbodiimide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

N-isopropyl-N'-phenylcarbodiimide (14041-89-5) + N-Cyclohexyl-N-hydroxy-N'-p-tolyl-formamidine (80820-90-2) → N-(4-methylphenyl)-N'-phenylurea (4300-33-8) + N-cyclohexyl-N'-isopropylcarbodiimide (3496-83-1)

Guidance literature:

In benzene; Yields of byproduct given; Ambient temperature;

DOI:10.1002/ardp.19813141206

Reference yield: 51.0%

dicyclohexyl-carbodiimide (538-75-0) + diisopropyl-carbodiimide (693-13-0) → N-cyclohexyl-N'-isopropylcarbodiimide (3496-83-1)

Guidance literature:

silica gel; chromium (II); In pentane; at 20 ℃; for 15h;

Reference yield:

N-cyclohexyl-N'-isopropylthiourea (34780-31-9) → N-cyclohexyl-N'-isopropylcarbodiimide (3496-83-1)

Guidance literature:

With calcium chloride; mercury(II) oxide; In acetone;

DOI:10.1016/S0022-328X(99)00142-4

upstream raw materials:

N-Isopropyl-N'-cyclohexyl-harnstoff

N-isopropyl-N'-phenylcarbodiimide

N-Cyclohexyl-N-hydroxy-N'-p-tolyl-formamidine

dicyclohexyl-carbodiimide

Downstream raw materials:

N¹-Isopropyl-N²-cyclohexyl-formamidin

Refernces

• 1、 Weiss, Karin,Hoffmann, Kurt. "Studies of Polymerisation and Metathesis Reactions, Part X. Polymerisation, Trimerisation and Metathesis of Allenes and Heteroallenes with Reduced Phillips Catalyst". . p. 769 - 773. Retrieved 2007/10/02.
• 2、 Zinner, Gerwalt,Schecker, Heinz-Guenther,Heuer, Wilhelm. "Reactions of N1-Hydroxyformamidines with Heterocumulenes". . p. 1006 - 1014. Retrieved 2007/10/02.