Technology Process of Fipexide
There total 1 articles about Fipexide which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Piperonylpiperazin, p-Chlorphenoxyessigsaeure, Pyridin;
- Guidance literature:
-
Fipexide;
With
bis(triphenylphosphine)carbonyliridium(I) chloride; 1,1,3,3-Tetramethyldisiloxane;
In
dichloromethane;
at 20 ℃;
for 0.333333h;
benzylmagnesium chloride;
at -78 - 20 ℃;
for 4h;
DOI:10.1039/c7sc03613b
- Guidance literature:
-
Fipexide;
With
bis(triphenylphosphine)iridium(I) carbonyl chloride;
In
toluene;
at 20 ℃;
for 0.0833333h;
With
1,1,3,3-Tetramethyldisiloxane;
In
toluene;
at 20 ℃;
for 0.0833333h;
With
trimethylsilyl cyanide;
In
toluene;
at 20 ℃;
for 0.5h;
DOI:10.1002/anie.201612367
