Technology Process of Bis(cyclopentadienyl)nickel(II)
There total 135 articles about Bis(cyclopentadienyl)nickel(II) which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
NaC5H5;
In
tetrahydrofuran;
byproducts: NH3; evolution of NH3 starts 35-40°C; slow heating to boiling;
- Guidance literature:
-
In
solid;
byproducts: TlCl; slight stoich. excess of NiCl2, stainless-steel vibration ball mill, 12 Hz, 6 min; sublimation (100-120°C, 0.1 Torr); elem. anal.;
DOI:10.1016/S0022-328X(99)00460-X
- Guidance literature:
-
With
NaC5H5; NH3;
In
tetrahydrofuran;
50°C, anhydrous NiCl2; 1 h;
