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3,4,7,8-Tetramethyl-1,10-phenanthroline

Base Information Edit
  • Chemical Name:3,4,7,8-Tetramethyl-1,10-phenanthroline
  • CAS No.:1660-93-1
  • Deprecated CAS:2408741-80-8
  • Molecular Formula:C16H16N2
  • Molecular Weight:236.316
  • Hs Code.:29339900
  • European Community (EC) Number:216-762-4
  • DSSTox Substance ID:DTXSID2061856
  • Nikkaji Number:J151.257I
  • Wikidata:Q72507689
  • ChEMBL ID:CHEMBL99384
  • Mol file:1660-93-1.mol
3,4,7,8-Tetramethyl-1,10-phenanthroline

Synonyms:3,4,7,8-tetramethyl-1,10-phenanthroline;TM-1,10-P

Suppliers and Price of 3,4,7,8-Tetramethyl-1,10-phenanthroline
Supply Marketing:Edit
Business phase:
The product has achieved commercial mass production*data from LookChem market partment
Manufacturers and distributors:
  • Manufacture/Brand
  • Chemicals and raw materials
  • Packaging
  • price
  • TRC
  • 3,4,7,8-Tetramethyl-1,10-phenanthroline
  • 1g
  • $ 70.00
  • TRC
  • 3,4,7,8-Tetramethyl-1,10-phenanthroline
  • 2.5g
  • $ 145.00
  • TCI Chemical
  • 3,4,7,8-Tetramethyl-1,10-phenanthroline >98.0%(HPLC)(T)
  • 5g
  • $ 141.00
  • TCI Chemical
  • 3,4,7,8-Tetramethyl-1,10-phenanthroline >98.0%(HPLC)(T)
  • 1g
  • $ 41.00
  • SynQuest Laboratories
  • 3,4,7,8-Tetramethyl-1,10-phenanthroline 95%
  • 25 g
  • $ 440.00
  • SynQuest Laboratories
  • 3,4,7,8-Tetramethyl-1,10-phenanthroline 95%
  • 5 g
  • $ 176.00
  • Sigma-Aldrich
  • 3,4,7,8-Tetramethyl-1,10-phenanthroline ≥98%
  • 1g
  • $ 84.10
  • Oakwood
  • 3,4,7,8-Tetramethyl-1,10-phenanthroline
  • 1g
  • $ 25.00
  • Oakwood
  • 3,4,7,8-Tetramethyl-1,10-phenanthroline
  • 250mg
  • $ 15.00
  • Oakwood
  • 3,4,7,8-Tetramethyl-1,10-phenanthroline
  • 5g
  • $ 70.00
Total 86 raw suppliers
Chemical Property of 3,4,7,8-Tetramethyl-1,10-phenanthroline Edit
Chemical Property:
  • Appearance/Colour:light beige fine crystalline powder 
  • Vapor Pressure:2.27E-07mmHg at 25°C 
  • Melting Point:277-280 °C(lit.) 
  • Refractive Index:1.662 
  • Boiling Point:435.2 °C at 760 mmHg 
  • PKA:6.37±0.10(Predicted) 
  • Flash Point:192.6 °C 
  • PSA:25.78000 
  • Density:1.129 g/cm3 
  • LogP:4.01660 
  • Storage Temp.:Sealed in dry,Room Temperature 
  • Solubility.:Soluble in 1,4-dioxane, acetone, dichloromethane, N,N-dimethylfo 
  • Water Solubility.:1.512mg/L(25.04 oC) 
  • XLogP3:3.9
  • Hydrogen Bond Donor Count:0
  • Hydrogen Bond Acceptor Count:2
  • Rotatable Bond Count:0
  • Exact Mass:236.131348519
  • Heavy Atom Count:18
  • Complexity:274
Purity/Quality:

99% *data from raw suppliers

3,4,7,8-Tetramethyl-1,10-phenanthroline *data from reagent suppliers

Safty Information:
  • Pictogram(s): HarmfulXn 
  • Hazard Codes:Xn 
  • Statements: 36/37/38-20/21/22-40 
  • Safety Statements: 36/37/39-26-36-22-24/25 
MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:
  • Chemical Classes:Other Classes -> Polycyclic Aromatic Hydrocarbons
  • Canonical SMILES:CC1=CN=C2C(=C1C)C=CC3=C(C(=CN=C32)C)C
  • Description 3,4,7,8-Tetramethyl-1,10-phenanthroline is used as a metal-chelating agent. For instance, it is used in the synthesis of heteroleptic cationic Ir(III) complex: 3,4,7,8-tetramethyl-1,10-phenanthroline-bis[2-(2’,4’-difluorophenyl)pyridine]iridium(III) hexafluorophosphate. It is used as a ligand to form dinuclear Cu(II) hypocrelin B complexes. It also forms tetraaqua(3,4,7,8-tetramethyl-1,10-phenanthroline-kappa2N,N′)zinc(II) thiosulfate complex with zinc.
  • Uses 3,4,7,8-Tetramethyl-1,10-phenanthroline is a metal-chelating agent.
Technology Process of 3,4,7,8-Tetramethyl-1,10-phenanthroline

There total 7 articles about 3,4,7,8-Tetramethyl-1,10-phenanthroline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With hydrogenchloride; at 80 ℃; for 16h;
Guidance literature:
With arsenic(V) oxide; sulfuric acid; at 100 - 140 ℃;
DOI:10.1021/ja01173a085
Guidance literature:
Multi-step reaction with 2 steps
1: SnCl2+2 H2O; ethanol
2: as2O5; aqueous H2SO4 / 100 - 140 °C
With arsenic(V) oxide; ethanol; sulfuric acid; tin(ll) chloride;
DOI:10.1021/ja01173a085
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