4-(Bis(2-hydroxyethyl)amino)azobenzene

Base Information

• Chemical Name: 4-(Bis(2-hydroxyethyl)amino)azobenzene
• CAS No.: 2452-84-8
• Molecular Formula: C16H19 N3 O2
• Molecular Weight: 285.346
• Hs Code.: 2927000090
• European Community (EC) Number: 607-394-9
• NSC Number: 260469
• UNII: 5YPY3R7L4G
• DSSTox Substance ID: DTXSID80871871
• Nikkaji Number: J33.603C
• Mol file: 2452-84-8.mol

Synonyms:C.I. SOLVENT YELLOW 58;2452-84-8;4-(Bis(2-hydroxyethyl)amino)azobenzene;2-[N-(2-hydroxyethyl)-4-phenyldiazenylanilino]ethanol;NSC 260469;NSC-260469;4-[Bis(2-hydroxyethyl)amino]azobenzene;Ethanol, 2,2'-[[4-(phenylazo)phenyl]imino]bis-;Ethanol, 2,2'-((4-(phenylazo)phenyl)imino)bis-;5YPY3R7L4G;SCHEMBL1615340;SCHEMBL9644455;DTXSID80871871;C.I. Solvent Yellow 58 (8CI);NSC260469;C.I.11129;N,N-Bis-hydroxyethyl-(4'-phenylazo)aniline;C.I. 11129;4-[N,N-bis (2-hydroxyethyl)-amino]azobenzene;Ethanol,2'-[[4-(phenylazo)phenyl]imino]bis-;2,2'-[[4-(2-Phenyldiazenyl)phenyl]imino]bis[ethanol];2-[(2-Hydroxyethyl)[4-(phenylazo)phenyl]amino]ethanol;Ethanol, 2,2'-[[4-(2-phenyldiazenyl)phenyl]imino]bis-;2,2'-{[4-(Phenyldiazenyl)phenyl]azanediyl}di(ethan-1-ol);Ethanol, 2,2'-[[4-[(1E)-2-phenyldiazeno]phenyl]imino]bis-;2-[(2-hydroxyethyl)({4-[(1E)-2-phenyldiazen-1-yl]phenyl})amino]ethan-1-ol

Chemical Property of 4-(Bis(2-hydroxyethyl)amino)azobenzene

Chemical Property:

• Vapor Pressure: 4.05E-11mmHg at 25°C
• Melting Point: 134°C
• Refractive Index: 1.6500 (estimate)
• Boiling Point: 507.4°Cat760mmHg
• Flash Point: 260.7°C
• PSA: 68.42000
• Density: 1.15g/cm³
• LogP: 2.89300
• Water Solubility.: 31.39mg/L(25 oC)
• XLogP3: 3.2
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 5
• Rotatable Bond Count: 7
• Exact Mass: 285.147726857
• Heavy Atom Count: 21
• Complexity: 292

Purity/Quality:

97% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Canonical SMILES: C1=CC=C(C=C1)N=NC2=CC=C(C=C2)N(CCO)CCO

Technology Process of 4-(Bis(2-hydroxyethyl)amino)azobenzene

There total 2 articles about 4-(Bis(2-hydroxyethyl)amino)azobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

benzenediazonium (2684-02-8) + 2,2'-(phenylimino)bis[ethanol] (120-07-0) → N,N-bis-(2-hydroxy-ethyl)-4-phenylazo-aniline (2452-84-8)

Guidance literature:

DOI:10.1039/jr9490001972

Reference yield:

→ N,N-bis-(2-hydroxy-ethyl)-4-phenylazo-aniline (2452-84-8)

Guidance literature:

/BRN= 762919/;

Reference yield: 100.0%

2-methyl-2-propenoic acid 2-hydroxyethyl ester (868-77-9,141668-69-1,25736-86-1,82601-55-6,25249-16-5) + poly(dimethylsiloxane-co-diphenylsiloxane) + N,N-bis-(2-hydroxy-ethyl)-4-phenylazo-aniline (2452-84-8) + isophorone diisocyanate (4098-71-9,101701-80-8,129212-17-5,149579-36-2,194936-84-0,26602-93-7,53895-32-2,66708-07-4,70936-97-9,74091-63-7,74520-92-6,102771-74-4,50974-99-7,52985-93-0) → polysiloxane (61790-90-7)

Guidance literature:

poly(dimethylsiloxane-co-diphenylsiloxane); N,N-bis-(2-hydroxy-ethyl)-4-phenylazo-aniline; isophorone diisocyanate; dibutyltin dilaurate; In dichloromethane; for 90h; Heating / reflux;

2-methyl-2-propenoic acid 2-hydroxyethyl ester; 1,1'-bi-2-naphthol; In dichloromethane; at 20 ℃; for 168h;

upstream raw materials:

benzenediazonium

2,2'-(phenylimino)bis[ethanol]

Downstream raw materials:

N,N-bis(2-chloroethyl)-4-(phenyldiazenyl)aniline

N-bis-(2-dimethylhydrosiloxyethyl)-(4-phenylazo)aniline

N,N-bis-(2-allylcarbamatoethyl)-(4'-phenylazo)aniline

N,N-bis-(2-vinylacetoxyethyl)-(4'-phenylazo)aniline

Refernces