Butyl ehtyl thionocarbamate

Base Information

• Chemical Name: Butyl ehtyl thionocarbamate
• CAS No.: 55365-85-0
• Molecular Formula: C7H15NOS
• Molecular Weight: 161.268
• Mol file: 55365-85-0.mol

Synonyms:Carbamothioic acid, butyl-, O-ethyl ester;

Chemical Property of Butyl ehtyl thionocarbamate

Chemical Property:

Purity/Quality:

95% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Butyl ehtyl thionocarbamate

There total 11 articles about Butyl ehtyl thionocarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 27.0%

N-(6,7-dimethoxy-2-methylquinazolin-3-io)-N-amide (74990-23-1) + N-butylamine (109-73-9,85404-21-3) → O-ethyl thiocarbamate (625-57-0) + O-Ethyl N-Butylthiocarbamate (55365-85-0) + 1-butyl-8,9-dimethoxy-5-methyl<1,2,4>-triazolo<5,1-a>quinazolinylium-2-olate + 1-butyl-8,9-dimethoxy-5-methyl<1,2,4>triazolo<5,1-a>quinazolinylium-2-thiolate

Guidance literature:

for 3h; Further byproducts given; Ambient temperature; Irradiation;

Reference yield: 12.0%

N-(6,7-dimethoxy-2-methylquinazolin-3-io)-N-amide (74990-23-1) + N-butylamine (109-73-9,85404-21-3) → O-ethyl thiocarbamate (625-57-0) + O-Ethyl N-Butylthiocarbamate (55365-85-0) + 3-butyl-6,7-dimethoxy-2-methylquinazoline-4(3H)-thione (92339-89-4) + 1-butyl-8,9-dimethoxy-5-methyl<1,2,4>triazolo<5,1-a>quinazolinylium-2-thiolate

Guidance literature:

for 3h; Further byproducts given; Ambient temperature; Irradiation;

Reference yield: 12.0%

N-(6,7-dimethoxy-2-methylquinazolin-3-io)-N-amide (74990-23-1) + N-butylamine (109-73-9,85404-21-3) → O-ethyl thiocarbamate (625-57-0) + O-Ethyl N-Butylthiocarbamate (55365-85-0) + 1-butyl-8,9-dimethoxy-5-methyl<1,2,4>triazolo<5,1-a>quinazolinylium-2-thiolate + 4-butylamino-6,7-dimethoxy-2-methylquinazoline (92339-86-1)

Guidance literature:

for 3h; Further byproducts given; Ambient temperature; Irradiation;

upstream raw materials:

N-(6,7-dimethoxy-2-methylquinazolin-3-io)-N-amide

N-butylamine

S-(ethoxycarbonyl) O-ethyl dithiocarbonate

methyl iodide

Downstream raw materials:

N,N'-ethylenethiourea

2-(2'-Aminoethylamino)-Δ²-imidazoline

Refernces

• 1、 Lempert-Sreter, Magda,Lempert, Karoly,Moeller, Joergen. "Electron Deficient Heteroaromatic Ammonioamidates. Part 26. N-(Quinazolin-3-io)amidates. Part 13. Phototransformations of an N-(Quinazolin-3-io)thioamidate and of a 10bH-1,3,4-thiadiazoloquinazoline, the Ring Isomer of an N-(Quinazolin-3-io)thioamidate, and the Photochemical Fo". . p. 1143 - 1152. Retrieved 2007/10/02.