Synthetic Communications p. 2695 - 2699 (1997)
Update date:2022-08-30
Topics:
Saravanan, Parthasarathy
Gupta, Suparna
DattaGupta, Arpita
Gupta, Sonia
Singh, Vinod K.
The cleavage of α-hydroxy tert-butyldimethylsilyl ether to diol takes place efficiently with LAH. It has been proposed that the reaction proceeds via intramolecular hydride transfer from the alkoxy aluminium hydride. In order to substantiate this, reduction of TBDMS ether with LAH in a variety of substrates was studied.
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Doi:10.1002/poc.1069
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(2013)Doi:10.1016/j.dyepig.2014.07.005
(2015)Doi:10.1016/S0040-4039(00)82864-6
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(2018)Doi:10.1016/S0040-4039(96)02391-X
(1997)