Synthesis p. 55 - 56 (1987)
Update date:2022-08-11
Topics:
Jousseaume, Bernard
Chanson, Evelyne
A new method of deoxygenation of amine oxides with tin reagent is proposed.It utilizes the reductive properties of the tin-tin bond in hexabutyldistannane or 1,2-dichlorotetrabutyldistannane.Oxides of tertiary amines are reduced into amines by hexabutyldistannane in high yields, whereas pyridine N-oxides react cleanly with 1,2-dichlorotetrabutyldistannane to give the corresponding pyridines.These reactions occur under mild conditions and are very selective.
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