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New Journal of Chemistry
DOI: 10.1039/C5NJ00801H
COMMUNICATION
Journal Name
9
6
.737 (s, 1H), 7.986 (s, 1H), 7.396ꢀ7.379 (d,
.765ꢀ6.748 (d, = 8.55, 2H); ESIꢀMS m/z 137 [M] .
J
= 8.55, 2H), 19 S. K. Maiti, S. Dinda, S. Banerjee, A. K. Mukherjee and R.
+
Bhattacharyya, Eur. J. Inorg. Chem., 2008, 2008, 2038–2051.
0 M. Brzaszcz, K. Kloc and J. Mlochowski, Polish J. Chem., 2003,
J
2
7
1 S. Tollari and F. Porta, J. Mol. Catal., 1993, 84, L137–L140.
HꢀNMR (500 MHz, DMSO): δ 11.51 (s, 1H), 8.80 (s, 22 S. K. Maiti, S. Banerjee, A. K. Mukherjee, K. M. Abdul Malik
7
, 1579–1586.
1
1. 1-Naphthaldehyde oxime (2n): white solid (0.091, 84%);
2
1
1
H), 8.68 (d,
J
=8.45 Hz, 1H), 7.95 (t,
J
=7.5, 7.65 Hz,
and R. Bhattacharyya, New J. Chem., 2005, 29, 554–563.
3 S. Tollari, S. Bruni, C. L. Bianchi, M. Rainoni and F. Porta, J.
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Tetrahedron, 1995, 51, 11305–11318.
2
2
2H), 7.81 (d,
J = 6.6 Hz, 1H), 7.63ꢀ7.49 (m, 3H); ESIꢀMS
+
m/z 171 [M] .
1
2. Cyclohexanone oxime (2p): white solid (0.104 g, 91%);
1
HꢀNMR (500 MHz, CDCl
t, 2H), 2.228ꢀ2.203 (t,
.05, 6H); ESIꢀMS m/z 113 [M] .
3
): δ 8.546 (s, 1H), 2.522ꢀ2.497 25 R. Joseph, T. Ravindranathan and A. Sudalai, Tetrahedron
Lett., 1995, 36, 1903–1904.
(
6
J = 6.0, 2H), 1.699ꢀ1.584 (m, J =
+
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1
27 W. D. Emmons, J. Am. Chem. Soc., 1954, 76, 3470–3472.
524.
Acknowledgements
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8 K. E. Gilbert and W. T. Borden, J. Org. Chem., 1979, 44, 659–
661.
Authors are thankful to Institute of Chemical technology and
UGCꢀCAS and UGCꢀGreen Tech, New Delhi for providing 29 S. K. Klitgaard, K. Egeblad, U. V Mentzel, A. G. Popov, T.
Jensen, E. Taarning, I. S. Nielsen and C. H. Christensen, Green
Chem., 2008, 10, 419–423.
financial assistance.
3
3
3
3
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| J. Name., 2012, 00, 1-3
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