Bulletin of the Chemical Society of Japan p. 2393 - 2399 (1995)
Update date:2022-08-04
Topics:
Hatsui
Wang
Takeshita
A mild base-catalyzed retro-benzilic acid rearrangement of a proto-photocycloadduct, formed in highly stereoselective photoaddition of methyl 2,4-dioxopentanoate to 1,5-dimethyl-6-methylene-1-cyclohexene, afforded a spiro[4.5]decenedione derivative. Reductive elimination of the α-dicarbonyl function and C1-homologation furnished (±)-hinesol and (±)-agarospirol.
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Doi:10.1016/0223-5234(96)88258-4
(1995)Doi:10.1016/S0040-4020(99)01091-1
(2000)Doi:10.1248/cpb.49.1581
(2001)Doi:10.1039/c4ob00922c
(2014)Doi:10.1039/c8gc00381e
(2018)Doi:10.1039/d0ra03323e
(2020)