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Name	9Z,12E-TETRADECADIENYL ACETATE	EINECS	N/A
CAS No.	30507-70-1	Density	0.89g/cm³
PSA	40.13000	LogP	3.76960
Solubility	N/A	Melting Point	N/A
Formula	C16H28 O2	Boiling Point	334.8°Cat760mmHg
Molecular Weight	252.397	Flash Point	102.3°C
Transport Information	N/A	Appearance	N/A
Safety	Moderately toxic by ingestion. When heated to decomposition it emits acrid smoke and irritating vapors.	Risk Codes	N/A
Molecular Structure		Hazard Symbols	N/A
Synonyms	9,12-Tetradecadien-1-ol,acetate, (9Z,12E)- (9CI); 9,12-Tetradecadien-1-ol, acetate, (E,Z)- (8CI);(Z,E)-9,12-Tetradecadienyl 1-acetate; (Z,E)-9,12-Tetradecadienyl acetate;(Z,E)-9,12-Tetradecadienyl acetate; 9Z,12E-Tetradecadienyl acetate; Litlure B;Prodenialure B; cis-9,trans-12-Tetradecadien-1-ol acetate;cis-9,trans-12-Tetradecadien-1-yl acetate; cis-9,trans-12-Tetradecadienylacetate	Article Data	24

9Z,12E-TETRADECADIENYL ACETATE Synthetic route

: 42521-46-0
Tetradeca-cis-9,trans-12-dien-1-ol

: 75-36-5
acetyl chloride

: 30507-70-1
Tetradec-9Z,12E-dien-1-yl Acetate

Conditions

Conditions	Yield
With pyridine In tetrahydrofuran	93%

: 42521-46-0
Tetradeca-cis-9,trans-12-dien-1-ol

: 108-24-7
acetic anhydride

A: 30507-70-1
Tetradec-9Z,12E-dien-1-yl Acetate

B: 58257-52-6
(Z)-undec-9-en-1-ol

Conditions

Conditions	Yield
With pyridine In dichloromethane at 20℃; for 18h; Inert atmosphere; chemoselective reaction;	A 89% B n/a

: 71394-01-9
(E)-12-tetradec-9-yn-12-en-1-yl acetate

: 30507-70-1
Tetradec-9Z,12E-dien-1-yl Acetate

Conditions

Conditions	Yield
With hydrogen; sodium tetrahydroborate; nickel diacetate; ethylenediamine In ethanol Ambient temperature;	85%
With quinoline; hydrogen; Lindlar's catalyst In hexane at -10℃;	55.5%
With hydrogen; P-2Ni
With quinoline; hydrogen; Lindlar's catalyst In hexane at -10℃; Yield given;

: 70654-44-3
(Z,E)-9,12-tetradecadien-1-ol

: 108-24-7
acetic anhydride

A: 30507-70-1
Tetradec-9Z,12E-dien-1-yl Acetate

B: 70654-47-6
(9E,12E)-tetradeca-9,12-dien-1-yl acetate

C: 51354-22-4
(Z,Z)-9,12-tetradecadienyl acetate

D: 31654-77-0
(9E,12Z)-9,12-tetradecadienyl acetate

Conditions

Conditions	Yield
In pyridine	A n/a B 83% C n/a D n/a

...Expand

: 112464-06-9
1-<(tetrahydro-2H-pyran-2-yl)oxy> 9Z, 12E-tetradecadiene

: 75-36-5
acetyl chloride

: 30507-70-1
Tetradec-9Z,12E-dien-1-yl Acetate

Conditions

Conditions	Yield
With pyridine In acetic acid for 12h; Ambient temperature;	79.3%
With pyridine; acetic acid	72%

: 112464-06-9
1-<(tetrahydro-2H-pyran-2-yl)oxy> 9Z, 12E-tetradecadiene

: 30507-70-1
Tetradec-9Z,12E-dien-1-yl Acetate

Conditions

Conditions	Yield
acetylation;	79%
Multi-step reaction with 2 steps 1: TsOH / methanol / Heating 2: pyridine View Scheme
Multi-step reaction with 2 steps 1: cc HCl / methanol / 5 h / Ambient temperature 2: 97 percent Chromat. / 4-dimethylaminopyridine / triethylamine View Scheme

: 112464-06-9
1-<(tetrahydro-2H-pyran-2-yl)oxy> 9Z, 12E-tetradecadiene

: 108-24-7
acetic anhydride

: 30507-70-1
Tetradec-9Z,12E-dien-1-yl Acetate

Conditions

Conditions	Yield
With titanium tetrachloride In dichloromethane at 0 - 25℃; for 6h; Acetylation;	78%

: 29541-97-7
9-acetoxynonal

: 120593-09-1
((E)-Pent-3-enylidene)-triphenyl-λ5-phosphane

: 30507-70-1
Tetradec-9Z,12E-dien-1-yl Acetate

Conditions

Conditions	Yield
at -78℃;	62%

: 29541-97-7
9-acetoxynonal

: 53143-96-7
<(E)-3-Pentenyl>triphenylphosphonium-bromid

: 30507-70-1
Tetradec-9Z,12E-dien-1-yl Acetate

Conditions

Conditions	Yield
Stage #1: <(E)-3-Pentenyl>triphenylphosphonium-bromid With sodium hexamethyldisilazane In tetrahydrofuran at -78℃; for 1h; Inert atmosphere; Stage #2: 9-acetoxynonal In tetrahydrofuran at -78 - 20℃; for 24h; Inert atmosphere;	56%
Stage #1: <(E)-3-Pentenyl>triphenylphosphonium-bromid With n-butyllithium; diisopropylamine In tetrahydrofuran; hexane at -20℃; for 1h; Stage #2: 9-acetoxynonal In tetrahydrofuran; hexane at -60 - 20℃; Wittig reaction; Further stages.;	54%

: 42521-46-0
Tetradeca-cis-9,trans-12-dien-1-ol

: 108-24-7
acetic anhydride

: 30507-70-1
Tetradec-9Z,12E-dien-1-yl Acetate

Conditions

Conditions	Yield
With pyridine Yield given;
With sodium acetate In neat (no solvent)

9Z,12E-TETRADECADIENYL ACETATE Chemical Properties

Product Name: 9Z,12E-Tetradecadienyl acetate (CAS NO.30507-70-1)

Molecular Formula: C₁₆H₂₈O₂
Molecular Weight: 252.3923 g/mol
Mol File: 30507-70-1.mol
Boiling point: 334.8 °C at 760 mmHg
Flash Point: 102.3 °C
Density: 0.89 g/cm³
Surface Tension: 30.8 dyne/cm
Enthalpy of Vaporization: 57.78 kJ/mol
Vapour Pressure: 0.000125 mmHg at 25°C
XLogP3-AA: 5.3
H-Bond Donor: 0
H-Bond Acceptor: 2

9Z,12E-TETRADECADIENYL ACETATE Toxicity Data With Reference

Organism	Test Type	Route	Reported Dose (Normalized Dose)	Effect	Source
mouse	LD50	oral	> 1gm/kg (1000mg/kg)		Japan Pesticide Information. Vol. (40), Pg. 32, 1982.
rat	LD50	oral	> 1gm/kg (1000mg/kg)		Japan Pesticide Information. Vol. (40), Pg. 32, 1982.

9Z,12E-TETRADECADIENYL ACETATE Consensus Reports

Reported in EPA TSCA Inventory.

9Z,12E-TETRADECADIENYL ACETATE Safety Profile

Moderately toxic by ingestion. When heated to decomposition it emits acrid smoke and irritating vapors.

9Z,12E-TETRADECADIENYL ACETATE Specification

9Z,12E-Tetradecadienyl acetate ,its CAS NO. is 30507-70-1,the synonyms is (2E,5Z)-14-Acetoxy-2,5-tetradecadiene ; (9Z,12E)-9,12-Tetradecadien-1-ol acetate ; Acetic acid (9Z,12E)-9,12-tetradecadienyl ester ; Acetic acid [(9Z,12E)-9,12-tetradecadienyl] ester ; Litlure B ; trans,cis-9,12-Tetradecadienyl acetate .

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