1255516-37-0Relevant articles and documents
Ultrasound-Assisted Preparation of Copper(I) Oxide Nanocubes: High Catalytic Activity in the Synthesis of Quinazolines
Raut, Amol B.,Tiwari, Abhishek R.,Bhanage, Bhalchandra M.
, p. 1292 - 1297 (2017)
A facile and green ultrasound-assisted synthesis of Cu2O nanocubes at room temperature is presented. The Cu2O nanocubes were characterized using XRD, SEM, TEM, energy-dispersive X-ray spectroscopy, UV/Vis spectroscopy, differential scanning calorimetry with thermogravimetric analysis, and FTIR spectroscopy. The Cu2O nanocubes were employed as a heterogeneous nanocatalyst and were found to be highly active in the preparation of quinazolines by the tandem cyclization of 2-bromobenzaldehydes with amidines under ligand-free conditions. Various quinazolines could be prepared in excellent yields within a very short reaction time. Furthermore, the Cu2O nanocatalyst could be recycled and reused up to four times without any significant loss of catalytic activity.
Copper-catalyzed synthesis of quinazoline derivatives via ullmann-type coupling and aerobic oxidation
Wang, Chen,Li, Shangfu,Liu, Hongxia,Jiang, Yuyang,Fu, Hua
supporting information; experimental part, p. 7936 - 7938 (2011/02/23)
A simple and efficient copper-catalyzed approach to quinazoline derivatives has been developed, and the protocol uses readily available substituted (2-bromophenyl)methylamines and amides as the starting materials, and the cascade reactions were performed