106310-21-8Relevant articles and documents
Development of Multigram Scale Synthesis of Trifluoromethylthiolating Reagent: (bpy)CuSCF3
Zhang, Yunxiao,Gan, Kangji,Weng, Zhiqiang
, p. 799 - 802 (2016)
A practical and reproducible procedure for the efficient preparation of (bpy)CuSCF3 (1), a copper reagent for trifluoromethylthiolation reaction, is reported. All reaction parameters were optimized, and reagent 1 was synthesized in 26 g scale.
Preparation method of 3-methyl-4-(4-trifluoromethylthio)benzoxy-nitrobenzene
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Paragraph 0008-0010, (2019/06/13)
The invention discloses a preparation method of 3-methyl-4-(4-trifluoromethylthio)benzoxy-nitrobenzene. 4-(trifluoromethylthio)phenol and 3-methyl-4-chloro-nitrobenzene are taken as starting materialsand dissolved in an organic solvent, condensation reaction is performed under the action of a catalyst, water is added for crystallization, and a product is obtained. The method is simple and convenient to operate, has high molar conversion rate and low production cost and is suitable for industrial production, and pollution control is greatly improved.
Method for synthesizing nitrobenzene ether from 2-amino-5-nitrotoluene
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Paragraph 0034; 0038; 0039; 0042, (2018/09/08)
The invention relates to the technical field of pharmaceutical synthesis and particularly relates to a method for synthesizing nitrobenzene ether from 2-amino-5-nitrotoluene. The method comprises thefollowing steps: reacting by virtue of 2-amino-5-nitroto