7-O-Acetyl-4-O-demethylpolysyphorin

Base Information

• Chemical Name: 7-O-Acetyl-4-O-demethylpolysyphorin
• CAS No.: 89706-39-8
• Molecular Formula: C₂₄H₃₀O₈
• Molecular Weight: 446.497
• Mol file: 89706-39-8.mol

Synonyms:

Chemical Property of 7-O-Acetyl-4-O-demethylpolysyphorin

Chemical Property:

Purity/Quality:

HPLC≥98% ^*data from raw suppliers

7-O-Acetyl-4-O-demethylpolysyphorin 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 7-O-Acetyl-4-O-demethylpolysyphorin

There total 4 articles about 7-O-Acetyl-4-O-demethylpolysyphorin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(E)-2,6,-dimethoxy-4-(prop-1-en-1-yl)phenol (20675-95-0) → threo-1-acetoxy-1-(4-hydroxy-3,5-dimethoxyphenyl)-2-<2,6-dimethoxy-4-(1-propenyl)phenoxy>propane (89706-39-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 100 percent / Ag₂O / benzene / 0.1 h / Ambient temperature

2: 210 mg / benzene / 0.33 h

With silver(l) oxide; In benzene;

Reference yield:

(E)-2,6,-dimethoxy-4-(prop-1-en-1-yl)phenol (20675-95-0) → erythro-1-acetoxy-1-(4-hydroxy-3,5-dimethoxyphenyl)-2-<2,6-dimethoxy-4-(1-propenyl)phenoxy>propane (89706-39-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 100 percent / Ag₂O / benzene / 0.1 h / Ambient temperature

2: 675 mg / benzene / 0.33 h

With silver(l) oxide; In benzene;

Reference yield:

acetic acid (64-19-7,77671-22-8) + 4-{2-[2,6-Dimethoxy-4-((E)-propenyl)-phenoxy]-propylidene}-2,6-dimethoxy-cyclohexa-2,5-dienone (89706-37-6) → threo-1-acetoxy-1-(4-hydroxy-3,5-dimethoxyphenyl)-2-<2,6-dimethoxy-4-(1-propenyl)phenoxy>propane (89706-39-8) + erythro-1-acetoxy-1-(4-hydroxy-3,5-dimethoxyphenyl)-2-<2,6-dimethoxy-4-(1-propenyl)phenoxy>propane (89706-39-8)

Guidance literature:

In benzene; for 0.333333h;

upstream raw materials:

acetic acid

4-{2-[2,6-Dimethoxy-4-((E)-propenyl)-phenoxy]-propylidene}-2,6-dimethoxy-cyclohexa-2,5-dienone

(E)-2,6,-dimethoxy-4-(prop-1-en-1-yl)phenol

Refernces