Technology Process of C45H77ClFN5O10P(1-)*Na(1+)
There total 5 articles about C45H77ClFN5O10P(1-)*Na(1+) which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
C57H106ClFN5O12PSi2;
With
tetrabutyl ammonium fluoride;
In
tetrahydrofuran;
for 4h;
With
hydrogenchloride;
In
methanol; chloroform; water;
pH=1;
With
sodium hydroxide;
In
methanol; water;
DOI:10.1016/j.bmc.2013.06.019
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: trifluoroacetic acid / tetrahydrofuran; water / 3 h / 0 °C
2.1: 1H-tetrazole / dichloromethane; acetonitrile / 24 h / Inert atmosphere
2.2: Inert atmosphere
3.1: pyridine; triethylamine / 24 h
4.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 4 h
4.2: pH 1
With
pyridine; 1H-tetrazole; tetrabutyl ammonium fluoride; triethylamine; trifluoroacetic acid;
In
tetrahydrofuran; dichloromethane; water; acetonitrile;
DOI:10.1016/j.bmc.2013.06.019
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: 1H-tetrazole / dichloromethane; acetonitrile / 24 h / Inert atmosphere
1.2: Inert atmosphere
2.1: pyridine; triethylamine / 24 h
3.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 4 h
3.2: pH 1
With
pyridine; 1H-tetrazole; tetrabutyl ammonium fluoride; triethylamine;
In
tetrahydrofuran; dichloromethane; acetonitrile;
DOI:10.1016/j.bmc.2013.06.019
