Technology Process of C47H74N2O15
There total 8 articles about C47H74N2O15 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 73 percent / triethylamine / CH2Cl2 / 5.5 h
2: 87 percent / (dimethylamino)pyridine (DMAP) / CH2Cl2 / 1.) -40 deg C, 1 h, 2.) -20 deg C, 72 h
3: 1.) sodium bis(trimethylsilyl)amide / 1.) THF, -35 deg C, 10 min, 2.) RT, 15 min
4: 94 percent / DBU / benzene / 22 h / Heating
5: 6 percent / CH2Cl2 / 5.5 h / 0 - 25 °C
6: MeOH / 96 h / Ambient temperature
With
methanol; dmap; sodium hexamethyldisilazane; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine;
In
dichloromethane; benzene;
DOI:10.1021/jo00245a038
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 87 percent / (dimethylamino)pyridine (DMAP) / CH2Cl2 / 1.) -40 deg C, 1 h, 2.) -20 deg C, 72 h
2: 1.) sodium bis(trimethylsilyl)amide / 1.) THF, -35 deg C, 10 min, 2.) RT, 15 min
3: 94 percent / DBU / benzene / 22 h / Heating
4: 6 percent / CH2Cl2 / 5.5 h / 0 - 25 °C
5: MeOH / 96 h / Ambient temperature
With
methanol; dmap; sodium hexamethyldisilazane; 1,8-diazabicyclo[5.4.0]undec-7-ene;
In
dichloromethane; benzene;
DOI:10.1021/jo00245a038
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 1.) sodium bis(trimethylsilyl)amide / 1.) THF, -35 deg C, 10 min, 2.) RT, 15 min
2: 94 percent / DBU / benzene / 22 h / Heating
3: 6 percent / CH2Cl2 / 5.5 h / 0 - 25 °C
4: MeOH / 96 h / Ambient temperature
With
methanol; sodium hexamethyldisilazane; 1,8-diazabicyclo[5.4.0]undec-7-ene;
In
dichloromethane; benzene;
DOI:10.1021/jo00245a038