Technology Process of C42H34N2O9S
There total 4 articles about C42H34N2O9S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C21H23NO4;
With
N-ethyl-N,N-diisopropylamine;
In
N,N-dimethyl-formamide;
for 0.166667h;
fluorescein-5-isothiocyanate;
In
N,N-dimethyl-formamide;
at 20 ℃;
Darkness;
DOI:10.1021/ml300191g
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: 200 °C
2.1: sodium sulfide nonahydrate; sodium hydrogensulfide / water / 24 h / Reflux
3.1: calcium carbonate / acetone / 3 h / 20 °C / Reflux
4.1: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 0.17 h
4.2: 20 °C / Darkness
With
sodium hydrogensulfide; sodium sulfide nonahydrate; N-ethyl-N,N-diisopropylamine; calcium carbonate;
In
water; N,N-dimethyl-formamide; acetone;
DOI:10.1021/ml300191g
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran / 20 °C
2.1: tetrabutyl-ammonium chloride; lithium chloride; lithium acetate; palladium diacetate / N,N-dimethyl-formamide / 100 °C
3.1: hydrogenchloride; water / tetrahydrofuran / 3 h / 60 °C
4.1: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 0.17 h
4.2: 20 °C / Darkness
With
hydrogenchloride; lithium acetate; tetrabutyl-ammonium chloride; water; palladium diacetate; N-ethyl-N,N-diisopropylamine; triphenylphosphine; lithium chloride; diethylazodicarboxylate;
In
tetrahydrofuran; N,N-dimethyl-formamide;
1.1: |Mitsunobu Displacement / 2.1: |Heck Reaction;
DOI:10.1021/ml300191g