DIETHYL (3,3-DIETHOXYPROPYL)PHOSPHONATE

Base Information

• Chemical Name: DIETHYL (3,3-DIETHOXYPROPYL)PHOSPHONATE
• CAS No.: 15110-17-5
• Molecular Formula: C11H25O5P
• Molecular Weight: 268.29
• Hs Code.: 29319019
• Mol file: 15110-17-5.mol

Synonyms:Phosphonicacid, (2-formylethyl)-, diethyl ester, diethyl acetal (7CI,8CI);Phosphonicacid, (3,3-diethoxypropyl)-, diethyl ester (9CI);Diethyl(3,3-diethoxypropyl)phosphonate;NSC 309693;

Chemical Property of DIETHYL (3,3-DIETHOXYPROPYL)PHOSPHONATE

Chemical Property:

• Appearance/Colour: Clear light yellow to orange liquid
• Vapor Pressure: 0.000239mmHg at 25°C
• Refractive Index: 1.429-1.432
• Boiling Point: 335 °C at 760 mmHg
• Flash Point: 170.2 °C
• PSA: 63.80000
• Density: 1.031 g/cm³
• LogP: 3.04170

Purity/Quality:

98% ^*data from raw suppliers

Diethyl (3,3-diethoxyprop-1-yl)phosphonate ^*data from reagent suppliers

Safty Information:

• Pictogram(s): Xi
• Hazard Codes: Xi
• Statements: 36/37/38
• Safety Statements: 37/39-26-24/25

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of DIETHYL (3,3-DIETHOXYPROPYL)PHOSPHONATE

There total 4 articles about DIETHYL (3,3-DIETHOXYPROPYL)PHOSPHONATE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

3-chloro-1,1-diethoxy-propane (35573-93-4) + triethyl phosphite (122-52-1) → diethyl 3,3-diethoxypropylphosphonate (15110-17-5)

Guidance literature:

Reference yield: 65.0%

3-bromopropinaldehyde diethyl acetal (59067-07-1) + triethyl phosphite (122-52-1) → diethyl 3,3-diethoxypropylphosphonate (15110-17-5)

Guidance literature:

at 170 ℃; for 1.5h;

DOI:10.1016/S0040-4020(01)92454-8

Reference yield:

3-chloro-1,1-diethoxy-propane (35573-93-4) + sodium diethyl phosphite (2303-76-6,118080-94-7) → diethyl 3,3-diethoxypropylphosphonate (15110-17-5)

Guidance literature:

In N,N-dimethyl-formamide;

upstream raw materials:

3-chloro-1,1-diethoxy-propane

sodium diethyl phosphite

triethyl phosphite

3-bromopropinaldehyde diethyl acetal

Refernces

• 1、 Varlet, J. M.,Fabre, G.,Sauveur, F.,Collignon, N.,Savignac, Ph.. "PREPARATION ET CONVERSION D'ω-FORMYLALKYLPHOSPHONATES EN ACIDES AMINOCARBOXYALKYLPHOSPHONIQUES". . p. 1377 - 1384. Retrieved 2007/10/02.