(C₆H₅NNC₅H₄N)HgCl₂

Base Information

• Chemical Name: (C₆H₅NNC₅H₄N)HgCl₂
• CAS No.: 61003-46-1
• Molecular Formula: C₁₁H₉Cl₂HgN₃
• Molecular Weight: 454.709
• Mol file: 61003-46-1.mol

Synonyms:

Chemical Property of (C₆H₅NNC₅H₄N)HgCl₂

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of (C₆H₅NNC₅H₄N)HgCl₂

There total 1 articles about (C₆H₅NNC₅H₄N)HgCl₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

(E)-2-(phenyldiazenyl)pyridine (54773-18-1) + mercury dichloride → (C6H5NNC5H4N)HgCl2 (61003-46-1)

Guidance literature:

In methanol; addn. of HgCl2 in hot MeOH to ligand in MeOH with constant stirring; refluxing for 1h; concg.; pptn.; washing (hexane); extn. (cold benzene); addn. of hexane to benzene; pptn.; elem. anal.;

Reference yield:

(C6H5NNC5H4N)HgCl2 (61003-46-1) + triphenylphosphine (603-35-0) → HgCl2(triphenylphosphine)2 (14494-85-0)

Guidance literature:

In acetone; byproducts: phenylazo-2-pyridine; treating complex with acetone soln. of P(C6H5)3; refluxing; IR;

upstream raw materials:

(E)-2-(phenyldiazenyl)pyridine

Downstream raw materials:

HgCl₂(triphenylphosphine)2