(8S,8'S)-(-)-secoisolariciresinol diglucoside

Base Information

• Chemical Name: (8S,8'S)-(-)-secoisolariciresinol diglucoside
• CAS No.: 257930-74-8
• Molecular Formula: C₃₂H₄₆O₁₆
• Molecular Weight: 686.708
• Mol file: 257930-74-8.mol

Synonyms:

Chemical Property of (8S,8'S)-(-)-secoisolariciresinol diglucoside

Chemical Property:

• Boiling Point: 989.2±65.0 °C(Predicted)
• Density: 1.52±0.1 g/cm3(Predicted)

Purity/Quality:

Analysis control,99.0% ^*data from raw suppliers

Secoisolariciresinol diglucoside 99.94% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (8S,8'S)-(-)-secoisolariciresinol diglucoside

There total 4 articles about (8S,8'S)-(-)-secoisolariciresinol diglucoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

C88H78O24 (1456548-37-0) → (8S,8'S)-(-)-secoisolariciresinol diglucoside (158932-33-3,257930-74-8)

Guidance literature:

With methanol; sodium methylate; at 25 ℃; for 60h; Inert atmosphere;

DOI:10.1016/j.bmcl.2013.07.062

Reference yield: 81.0%

C88H78O24 (1456548-38-1) → secoisolariciresinol diglycoside (158932-33-3,257930-74-8)

Guidance literature:

With methanol; sodium methylate; at 25 ℃; for 60h; Inert atmosphere;

DOI:10.1016/j.bmcl.2013.07.062

Reference yield:

C88H78O24 → (8S,8'S)-(-)-secoisolariciresinol diglucoside (158932-33-3,257930-74-8) + secoisolariciresinol diglycoside (158932-33-3,257930-74-8)

Guidance literature:

With methanol; sodium methylate; at 5 - 20 ℃; for 40.5h; Overall yield = ~ 100 g; Inert atmosphere;

upstream raw materials:

C₈₈H₇₈O₂₄

C₈₈H₇₈O₂₄

Refernces

• 1、 -. "PREPARATION OF (S,S)-SECOISOLARICIRESINOL DIGLUCOSIDE AND (R,R)-SECOISOLARICIRESINOL DIGLUCOSIDE". Paragraph 00141; 00145. . Retrieved 2015/01/09.