2-Cyano-3-(2,6-dimethyl-phenylamino)-but-2-enedinitrile

Base Information Edit

Chemical Name:2-Cyano-3-(2,6-dimethyl-phenylamino)-but-2-enedinitrile
CAS No.:108954-75-2
Molecular Formula:C₁₃H₁₀N₄
Molecular Weight:222.249
Hs Code.:
Mol file:108954-75-2.mol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-Cyano-3-(2,6-dimethyl-phenylamino)-but-2-enedinitrile Edit

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Technology Process of 2-Cyano-3-(2,6-dimethyl-phenylamino)-but-2-enedinitrile

There total 5 articles about 2-Cyano-3-(2,6-dimethyl-phenylamino)-but-2-enedinitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3189-44-4
2,2,1-tricyano-1-hydroxy-ethylene, tetramethyl-ammonium salt

: 108954-75-2
2-Cyano-3-(2,6-dimethyl-phenylamino)-but-2-enedinitrile

Guidance literature:: Multi-step reaction with 2 steps

1: oxalyl bromide / diethyl ether; 1,2-dimethoxy-ethane / 1 h / 5 °C

2: CHCl₃ / 32 °C / other temperatures

With Oxalyl bromide; In 1,2-dimethoxyethane; diethyl ether; chloroform;
DOI:10.1016/S0040-4039(01)91164-5