N1,N10-Bis(p-coumaroyl)spermidine

Base Information

• Chemical Name: N1,N10-Bis(p-coumaroyl)spermidine
• CAS No.: 114916-05-1
• Molecular Formula: C25H31 N3 O4
• Molecular Weight: 437.53100
• Mol file: 114916-05-1.mol

Synonyms:N1,N10-Bis(p-coumaroyl)spermidine

Chemical Property of N1,N10-Bis(p-coumaroyl)spermidine

Chemical Property:

• PSA: 110.69000
• LogP: 3.98940

Purity/Quality:

98%min ^*data from raw suppliers

N1,N10-Bis(p-coumaroyl)spermidine 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of N1,N10-Bis(p-coumaroyl)spermidine

There total 17 articles about N1,N10-Bis(p-coumaroyl)spermidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

{4-[(E)-3-(4-Methoxy-phenyl)-acryloylamino]-butyl}-{3-[(E)-3-(4-methoxy-phenyl)-acryloylamino]-propyl}-carbamic acid tert-butyl ester → N,N′-di-p-coumaroylspermidine (114916-05-1)

Guidance literature:

With boron tribromide; In tetrahydrofuran; at -78 ℃; for 1h;

DOI:10.1016/S0040-4020(98)01014-X

Reference yield: 48.6%

C34H43N3O8 → N,N′-di-p-coumaroylspermidine (114916-05-1)

Guidance literature:

With potassium carbonate; In methanol; at 20 ℃; for 2h;

DOI:10.1093/bbb/zbab223

Reference yield:

(E)-3-[4-(tert-Butyl-dimethyl-silanyloxy)-phenyl]-N-[3-(4-{(E)-3-[4-(tert-butyl-dimethyl-silanyloxy)-phenyl]-acryloylamino}-butylamino)-propyl]-acrylamide → N,N′-di-p-coumaroylspermidine (114916-05-1)

Guidance literature:

With tetrabutyl ammonium fluoride; In tetrahydrofuran; for 1h; Ambient temperature;

DOI:10.1016/S0031-9422(97)00590-6

upstream raw materials:

N-(3-aminopropyl)-1,4-diaminobutane

(E)-3-(4'-((tert-butyldimethylsilyl)oxy)phenyl)acrylic acid

(E)-3-(4-methoxyphenyl)acrylic acid

(E)-3-(4-methoxyphenyl)propenoyl chloride

Refernces

• 1、 Asami, Tadao,Ota, Tsuyoshi,Takahashi, Ikuo. "Function of hydroxycinnamoyl spermidines in seedling growth of Arabidopsis". . p. 294 - 299. Retrieved 2022/03/15.
• 2、 Sagner, Silvia,Shen, Zheng-Wu,Deus-Neumann, Brigitte,Zenk, Meinhart H.. "The biosynthesis of lunarine in seeds of Lunaria annua". . p. 375 - 387. Retrieved 2007/10/03.