C₁₀₃H₉₀N₂₂O₃₉P₂

Base Information

• Chemical Name: C₁₀₃H₉₀N₂₂O₃₉P₂
• CAS No.: 153120-98-0
• Molecular Formula: C₁₀₃H₉₀N₂₂O₃₉P₂
• Molecular Weight: 2321.92
• Mol file: 153120-98-0.mol

Synonyms:

Chemical Property of C₁₀₃H₉₀N₂₂O₃₉P₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₀₃H₉₀N₂₂O₃₉P₂

There total 2 articles about C₁₀₃H₉₀N₂₂O₃₉P₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.0%

fluoresceinamine (3326-34-9) + 2'-deoxy-N6,5'-O-bis{[2-(4-nitrophenyl)ethoxy]carbonyl}adenylyl-{3'-{OP-[2-(4-nitrophenyl)ethyl]}-5'}-2'-deoxy-N6-(phenoxycarbonyl)adenylyl-{3'-{OP-[2-(4-nitrophenyl)ethyl]}-5'}-2'-deoxy-N6,3'-O-bis{[2-(4-nitrophenyl)ethoxy]carbonyl}adenosine → C103H90N22O39P2 (153120-98-0)

Guidance literature:

In pyridine; at 60 - 70 ℃; for 2h;

DOI:10.1002/hlca.200390186

Reference yield:

fluoresceinamine (3326-34-9) + C97H89N21O35P2 (153120-96-8) → C103H90N22O39P2 (153120-98-0)

Guidance literature:

With phenoxycarbonyltetrazolide; triethylamine; Multistep reaction;

DOI:10.1080/07328319708002935

upstream raw materials:

fluoresceinamine

C₉₇H₈₉N₂₁O₃₅P₂

Refernces

• 1、 Sigmund, Harald,Maier, Thomas,Pfleiderer, Wolfgang. "A new type of fluorescence labeling of nucleosides, nucleotides and oligonucleotides". . p. 685 - 696. Retrieved 2007/10/03.