N,N-diethyl-N'-(2-phenyl-[4]quinolylmethyl)-propanediyldiamine

Base Information

• Chemical Name: N,N-diethyl-N'-(2-phenyl-[4]quinolylmethyl)-propanediyldiamine
• CAS No.: 47492-97-7
• Molecular Formula: C₂₃H₂₉N₃
• Molecular Weight: 347.503
• Mol file: 47492-97-7.mol

Synonyms:

Chemical Property of N,N-diethyl-N'-(2-phenyl-[4]quinolylmethyl)-propanediyldiamine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N,N-diethyl-N'-(2-phenyl-[4]quinolylmethyl)-propanediyldiamine

There total 6 articles about N,N-diethyl-N'-(2-phenyl-[4]quinolylmethyl)-propanediyldiamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-[3-(diethylamino)propyl]-2-phenylquinoline-4-carboxamide → N,N-diethyl-N'-(2-phenyl-[4]quinolylmethyl)-propanediyldiamine (47492-97-7)

Guidance literature:

With chloroform; phosphorus pentachloride; Behandeln des Reaktionsprodukts mit SnCl₂ und HCl in Aether;

DOI:10.1021/ja01225a055

Reference yield:

C6H4NCH2CHCCH2 (491-35-0) → N,N-diethyl-N'-(2-phenyl-[4]quinolylmethyl)-propanediyldiamine (47492-97-7)

Guidance literature:

Multi-step reaction with 3 steps

1: diethyl ether

2: selenium dioxide; dioxane

3: platinum; ethanol / Hydrogenation

With 1,4-dioxane; selenium(IV) oxide; diethyl ether; ethanol; platinum;

DOI:10.1021/ja01225a055

Reference yield:

ethyl 2-phenylquinoline-4-carboxylate (4420-46-6) → N,N-diethyl-N'-(2-phenyl-[4]quinolylmethyl)-propanediyldiamine (47492-97-7)

Guidance literature:

Multi-step reaction with 2 steps

1: anschliessend Erhitzen des Reaktionsgemisches auf 140-150grad unter Abdestillieren des entstandenen Aethanols

2: PCl₅; CHCl₃ / Behandeln des Reaktionsprodukts mit SnCl₂ und HCl in Aether

With chloroform; phosphorus pentachloride;

DOI:10.1021/ja01225a055

upstream raw materials:

2-phenyl-4-quinolinecarboxaldehyde

diethylaminopropylamine

C₆H₄NCH₂CHCCH₂

ethyl 2-phenylquinoline-4-carboxylate