2,4-Dimethoxyphenylmagnesium bromide

Base Information

• Chemical Name: 2,4-Dimethoxyphenylmagnesium bromide
• CAS No.: 138109-49-6
• Molecular Formula: C8H9BrMgO2
• Molecular Weight: 241.367
• Hs Code.: 2827310000
• Mol file: 138109-49-6.mol

Synonyms:2,4-DIMETHOXYPHENYLMAGNESIUM BROMIDE;2,4-DIMETHOXYPHENYLMAGNESIUM BROMIDE, 0.5M SOLUTION IN TETRAHYDROFURAN;2,4-dimethoxyphenylmagnesium bromide solution;2,4-Dimethoxyphenylmagnesium bromide solution 0.5 in THF;2,4-DiMethoxyphenylMagnesiuM broMide, 0.5M in 2-MeTHF;2,4-Dimethoxyphenylmagnesium bromide 0.5M solution in THF

Chemical Property of 2,4-Dimethoxyphenylmagnesium bromide

Chemical Property:

• Vapor Pressure: 0.195mmHg at 25°C
• Refractive Index: ">
• Boiling Point: 65 °C
• Flash Point: 1 °F
• PSA: 18.46000
• Density: 0.960 g/mL at 25 °C
• LogP: 2.34960
• Storage Temp.: 2-8°C

Purity/Quality:

98%Min ^*data from raw suppliers

2,4-Dimethoxyphenylmagnesium bromide solution 0.5M in THF ^*data from reagent suppliers

Safty Information:

• Pictogram(s): F,C
• Hazard Codes: F,C,Xn
• Statements: 11-14-19-34-40-36/37
• Safety Statements: 16-29-33-45-36/37-26

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2,4-Dimethoxyphenylmagnesium bromide

There total 3 articles about 2,4-Dimethoxyphenylmagnesium bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-Bromo-2,4-dimethoxybenzene (17715-69-4) → 2,4-dimethoxyphenylmagnesium bromide (138109-49-6)

Guidance literature:

With iodine; magnesium; In tetrahydrofuran; at 0 ℃; for 0.5h;

DOI:10.1002/chem.201703686

Reference yield:

1-Bromo-2,4-dimethoxybenzene (17715-69-4) → 2,4-dimethoxyphenylmagnesium bromide (138109-49-6)

Guidance literature:

In tetrahydrofuran;

Reference yield:

→ 2,4-dimethoxyphenylmagnesium bromide (138109-49-6)

Guidance literature:

upstream raw materials:

1-Bromo-2,4-dimethoxybenzene

Downstream raw materials:

Osmorhizole

11β-(2,4-dimethoxyphenyl)-3,3-<2,2-dimethyl-1,3-propanediylbis(oxy)>-5α-estr-9-ene-5,17β-diol

(+/-)-N-(2'-fluorophenyl)-2-(α-hydroxy-2',4'-dimethoxybenzyl)pyrrole

[2-(2,4-Dimethoxyphenyl)-6-methoxybenzo[b]thien-3-yl] [4-[2-(1-piperidinyl)ethoxy]phenyl]methanone

Refernces

• 1、 -. "ENDOTHELIN RECEPTOR ANTAGONISTS". . . Retrieved 2008/06/13.