Technology Process of C39H45NO8
There total 6 articles about C39H45NO8 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
2,6-di-tert-butyl-4-methyl-phenol; tetrabutylammomium bromide;
In
acetonitrile;
for 16h;
Reflux;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: tetra(n-butyl)ammonium hydrogensulfate; potassium hydroxide / acetone / 16 h / Reflux
2: aluminum (III) chloride / dichloromethane / 15 h / 20 - 30 °C
3: aluminum (III) chloride / dichloromethane / 48 h / 20 - 30 °C
4: sodium hydroxide / ethanol / 3 h / 50 °C
5: 2,6-di-tert-butyl-4-methyl-phenol; tetrabutylammomium bromide / acetonitrile / 16 h / Reflux
With
2,6-di-tert-butyl-4-methyl-phenol; tetrabutylammomium bromide; tetra(n-butyl)ammonium hydrogensulfate; potassium hydroxide; sodium hydroxide;
aluminum (III) chloride;
In
ethanol; dichloromethane; acetone; acetonitrile;
2: Friedel Crafts Acylation / 3: Friedel Crafts Acylation;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: aluminum (III) chloride / dichloromethane / 15 h / 20 - 30 °C
2: aluminum (III) chloride / dichloromethane / 48 h / 20 - 30 °C
3: sodium hydroxide / ethanol / 3 h / 50 °C
4: 2,6-di-tert-butyl-4-methyl-phenol; tetrabutylammomium bromide / acetonitrile / 16 h / Reflux
With
2,6-di-tert-butyl-4-methyl-phenol; tetrabutylammomium bromide; sodium hydroxide;
aluminum (III) chloride;
In
ethanol; dichloromethane; acetonitrile;
1: Friedel Crafts Acylation / 2: Friedel Crafts Acylation;
