chrysin-ethylidene-sparfloxacin

Base Information

• Chemical Name: chrysin-ethylidene-sparfloxacin
• CAS No.: 1517965-84-2
• Molecular Formula: C₃₆H₃₄F₂N₄O₇
• Molecular Weight: 672.685
• Mol file: 1517965-84-2.mol

Synonyms:chrysin-ethylidene-sparfloxacin

Chemical Property of chrysin-ethylidene-sparfloxacin

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of chrysin-ethylidene-sparfloxacin

There total 2 articles about chrysin-ethylidene-sparfloxacin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 36.0%

7-(2-bromoethoxy)-5-hydroxy-2-phenyl-4H-chromen-4-one (41988-26-5) + sparfloxacin (110871-86-8) → chrysin-ethylidene-sparfloxacin (1517965-84-2)

Guidance literature:

With dmap; In dimethyl sulfoxide; at 60 ℃;

DOI:10.1016/j.ejmech.2014.04.037

Reference yield:

5,7-dihydroxy-2-phenyl-chromen-4-one (480-40-0) → chrysin-ethylidene-sparfloxacin (1517965-84-2)

Guidance literature:

Multi-step reaction with 2 steps

1: potassium carbonate / N,N-dimethyl-formamide / 70 °C

2: dmap / dimethyl sulfoxide / 60 °C

With dmap; potassium carbonate; In dimethyl sulfoxide; N,N-dimethyl-formamide;

DOI:10.1016/j.ejmech.2014.04.037

upstream raw materials:

5,7-dihydroxy-2-phenyl-chromen-4-one

7-(2-bromoethoxy)-5-hydroxy-2-phenyl-4H-chromen-4-one

sparfloxacin

Refernces