Technology Process of C16H13BrFN3O4S
There total 6 articles about C16H13BrFN3O4S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
methanol; potassium carbonate;
at 20 ℃;
for 0.5h;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: water; lithium hydroxide / tetrahydrofuran; methanol / 2 h / 70 °C / Inert atmosphere
1.2: 0 °C / pH 6
2.1: diphenyl phosphoryl azide; triethylamine / 6 h / 90 °C / Inert atmosphere
3.1: N,N-dimethyl-formamide / 42 h / 80 °C / Inert atmosphere
3.2: 0.25 h / 0 °C
4.1: hydrogenchloride / 1,4-dioxane / 3 h / 20 °C
5.1: pyridine / 1.5 h / 0 - 20 °C
6.1: methanol; potassium carbonate / 0.5 h / 20 °C
With
pyridine; hydrogenchloride; methanol; diphenyl phosphoryl azide; water; potassium carbonate; triethylamine; lithium hydroxide;
In
tetrahydrofuran; 1,4-dioxane; methanol; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: N,N-dimethyl-formamide / 42 h / 80 °C / Inert atmosphere
1.2: 0.25 h / 0 °C
2.1: hydrogenchloride / 1,4-dioxane / 3 h / 20 °C
3.1: pyridine / 1.5 h / 0 - 20 °C
4.1: methanol; potassium carbonate / 0.5 h / 20 °C
With
pyridine; hydrogenchloride; methanol; potassium carbonate;
In
1,4-dioxane; N,N-dimethyl-formamide;