(MeO)2Tr-OAc

Base Information Edit

Chemical Name:(MeO)2Tr-OAc
CAS No.:1254223-76-1
Molecular Formula:C₂₃H₂₂O₄
Molecular Weight:362.425
Hs Code.:
Mol file:1254223-76-1.mol

Synonyms:(MeO)2Tr-OAc

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Chemical Property of (MeO)2Tr-OAc Edit

Chemical Property:

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Technology Process of (MeO)2Tr-OAc

There total 2 articles about (MeO)2Tr-OAc which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 108-24-7
acetic anhydride

: 40615-35-8
4,4'-dimethoxytrityl alcohol

: 1254223-76-1
(MeO)2Tr-OAc

Guidance literature:: at 80 ℃; Cooling with ice;
DOI:10.1016/j.bmcl.2010.12.098

Reference yield:

: bis(4-methoxyphenyl)phenylmethylium tetrafluoroborate

: 10534-59-5
tetrabutylammonium acetate

: 1254223-76-1
(MeO)2Tr-OAc

Guidance literature:: DOI:10.1002/chem.200902669

Reference yield:

: 1254223-76-1
(MeO)2Tr-OAc

: 40615-39-2
5'-O-(4-4'-dimethoxytrityl)thymidine

Guidance literature:: Multi-step reaction with 2 steps

1: tetrafluoroboric acid / water / 0.67 h / Cooling with ice

2: lithium carbonate; N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 20 °C / Heating

With tetrafluoroboric acid; lithium carbonate; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; water;
DOI:10.1016/j.bmcl.2010.12.098