GLYCYL-DL-ASPARAGINE

Base Information

• Chemical Name: GLYCYL-DL-ASPARAGINE
• CAS No.: 32729-21-8
• Molecular Formula: C6H11 N3 O4
• Molecular Weight: 189.171
• Hs Code.: 2924199090
• Mol file: 32729-21-8.mol

Synonyms:Asparagine,N2-glycyl-; Asparagine, N2-glycyl-, DL- (8CI); DL-Asparagine, N2-glycyl- (6CI);Glycyl-DL-asparagine

Chemical Property of GLYCYL-DL-ASPARAGINE

Chemical Property:

• Boiling Point: 628.2±55.0 °C(Predicted)
• PKA: 2.94±0.10(Predicted)
• PSA: 135.51000
• Density: 1.422±0.06 g/cm3(Predicted)
• LogP: -0.81860
• Water Solubility.: almost transparency

Purity/Quality:

98%,99%, ^*data from raw suppliers

H-GLY-DL-ASN-OH ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Uses: H-GLY-DL-ASN-OH is a chiral resolution of dipeptides by ligand exchange chromatography on chemically bonded chiral phases.

Technology Process of GLYCYL-DL-ASPARAGINE

There total 2 articles about GLYCYL-DL-ASPARAGINE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ glycyl-DL-asparagine (32729-21-8,24667-21-8)

Guidance literature:

With ammonia; water; at 100 ℃; glycyl-l-asparagine;

Reference yield:

N2-(N,N-phthaloyl-glycyl)-DL-asparagine (35181-18-1) → glycyl-DL-asparagine (32729-21-8,24667-21-8)

Guidance literature:

With hydrazine;

Reference yield: 95.0%

glycyl-DL-asparagine (32729-21-8,24667-21-8) → glycyl-DL-aspartic acid (79731-35-4)

Guidance literature:

With Amberlyst 15; water; at 100 ℃; for 24h;

DOI:10.1021/jo00339a019

upstream raw materials:

N²-(N,N-phthaloyl-glycyl)-DL-asparagine

Downstream raw materials:

N-chloroacetyl-DL-aspartic acid

glycyl-DL-aspartic acid