2,3-dihydro-4-phenylthiophene

Base Information Edit

Chemical Name:2,3-dihydro-4-phenylthiophene
CAS No.:99059-46-8
Molecular Formula:C₁₀H₁₀S
Molecular Weight:162.255
Hs Code.:
Mol file:99059-46-8.mol

Synonyms:2,3-dihydro-4-phenylthiophene

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Chemical Property of 2,3-dihydro-4-phenylthiophene Edit

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Technology Process of 2,3-dihydro-4-phenylthiophene

There total 2 articles about 2,3-dihydro-4-phenylthiophene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1003-04-9
Tetrahydrothiophen-3-one

: phenylmagnesium bromide

: 99059-46-8
2,3-dihydro-4-phenylthiophene

Guidance literature:: With diethyl ether; Erhitzen des erhaltenen 3-Phenyl-tetrahydro-thiophen-3-ols mit Kaliumhydrogensulfat oder mit wss. Schwefelsaeure;
DOI:10.1021/ja01565a058

Reference yield:

: 930-69-8
sodium thiophenolate

: 99059-46-8
2,3-dihydro-4-phenylthiophene

Guidance literature:: Multi-step reaction with 2 steps

1: benzene / 4 h / Heating

2: 1.) Bu₃SnH, AIBN, 2.) CH₃OD, AcOD / 1.) benzene, reflux, 30 min, 2.) r.t., 3 days

With 2,2'-azobis(isobutyronitrile); deuteromethanol; deuteroacetic acid; tri-n-butyl-tin hydride; In benzene;
DOI:10.1021/jo00091a025