Bromobenzene;iodozinc(1+)

Base Information

• Chemical Name: Bromobenzene;iodozinc(1+)
• CAS No.: 186000-44-2
• Molecular Formula: C₆H₄BrIZn
• Molecular Weight: 348.296
• DSSTox Substance ID: DTXSID00400127
• Mol file: 186000-44-2.mol

Synonyms:bromobenzene;iodozinc(1+);186000-44-2;DTXSID00400127

Chemical Property of Bromobenzene;iodozinc(1+)

Chemical Property:

• Vapor Pressure: 4.12mmHg at 25°C
• Boiling Point: 65℃
• Flash Point: 1℉
• PSA: 0.00000
• Density: 1.023g/mLat25℃
• LogP: 3.13250
• Storage Temp.: 2-8°C
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 0
• Exact Mass: 345.78325
• Heavy Atom Count: 9
• Complexity: 142

Purity/Quality:

98%,99%, ^*data from raw suppliers

3-Bromophenylzinc iodide solution 0.5M in THF ^*data from reagent suppliers

Safty Information:

• Hazard Codes: F,Xn
• Statements: 11-14-19-22-36/37/38-40-36/37
• Safety Statements: 16-26-33-36-36/37

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

• Canonical SMILES: C1=C[C-]=CC(=C1)Br.[Zn+]I

Technology Process of Bromobenzene;iodozinc(1+)

There total 1 articles about Bromobenzene;iodozinc(1+) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-Bromo-3-iodobenzene (591-18-4) + zinc (7440-66-6) → (3-bromophenyl)zinc (II) iodide (186000-44-2)

Guidance literature:

zinc; With lithium chloride; at 150 - 170 ℃; for 2h; Schlenk technique; Inert atmosphere;

With chloro-trimethyl-silane; ethylene dibromide; In tetrahydrofuran; at 20 ℃; for 0.0833333h; Glovebox; Schlenk technique; Inert atmosphere;

1-Bromo-3-iodobenzene; In tetrahydrofuran; Glovebox; Schlenk technique; Inert atmosphere;

DOI:10.1002/anie.201913435

upstream raw materials:

1-Bromo-3-iodobenzene

zinc

Refernces