2-Nitrophenyl2,3,4-tri-O-acetyl-b-D-xylopyranoside

Base Information

• Chemical Name: 2-Nitrophenyl2,3,4-tri-O-acetyl-b-D-xylopyranoside
• CAS No.: 10256-24-3
• Molecular Formula: C17H19 N O10
• Molecular Weight: 397.339
• Mol file: 10256-24-3.mol

Synonyms:Xylopyranoside,o-nitrophenyl, 2',3',4'-triacetate, b-D- (7CI,8CI)

Chemical Property of 2-Nitrophenyl2,3,4-tri-O-acetyl-b-D-xylopyranoside

Chemical Property:

• Melting Point: 105-107°C
• PSA: 143.18000
• LogP: 1.64820
• Storage Temp.: -20°C Freezer
• Solubility.: Chloroform (Slightly), Ethyl Acetate (Slightly)

Purity/Quality:

98%,99%, ^*data from raw suppliers

2’-Nitrophenyl2,3,4-Tri-O-acetyl-β-D-xylopyranoside ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Uses: 2’-Nitrophenyl 2,3,4-Tri-O-acetyl-β-D-xylopyranoside (cas# 10256-24-3) is a compound useful in organic synthesis.

Technology Process of 2-Nitrophenyl2,3,4-tri-O-acetyl-b-D-xylopyranoside

There total 2 articles about 2-Nitrophenyl2,3,4-tri-O-acetyl-b-D-xylopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

2-hydroxynitrobenzene (88-75-5,78813-12-4) + 1-bromo-2,3,4-tri-O-acetyl-α-D-xylopyranose (3068-31-3) → o-nitrophenyl 2,3,4,6-tetra-O-acetyl-β-D-xylopyranoside (10256-24-3)

Guidance literature:

With potassium carbonate; In acetone; Ambient temperature;

DOI:10.1016/0008-6215(95)00214-E

Reference yield:

→ o-nitrophenyl 2,3,4,6-tetra-O-acetyl-β-D-xylopyranoside (10256-24-3)

Guidance literature:

aus 2-Nitro-phenol u. O².O³.O⁴-Triacetyl-α-D-xylopyranosylbromid;

DOI:10.1007/BF00637877

Reference yield: 92.0%

o-nitrophenyl 2,3,4,6-tetra-O-acetyl-β-D-xylopyranoside (10256-24-3) → 2-nitrophenyl β-D-xylopyranoside (10238-27-4)

Guidance literature:

With methanol; sodium methylate; for 5h; Ambient temperature;

DOI:10.1016/0008-6215(95)00214-E

upstream raw materials:

2-hydroxynitrobenzene

1-bromo-2,3,4-tri-O-acetyl-α-D-xylopyranose

Downstream raw materials:

2-nitrophenyl β-D-xylopyranoside

2-nitrophenyl O-β-D-xylopyranosyl-(1<*>4)-β-D-xylopyranoside

2-nitrophenyl 2,3-di-O-benzoyl-β-D-xylopyranoside

2-nitrophenyl 2,3-di-O-benzoyl-4-O-chloroacetyl-β-D-xylopyranoside

Refernces