3,4-Dimethylphenylhydrazine hydrochloride

Base Information

• Chemical Name: 3,4-Dimethylphenylhydrazine hydrochloride
• CAS No.: 13636-53-8
• Molecular Formula: C8H12 N2
• Molecular Weight: 136.197
• Mol file: 13636-53-8.mol

Synonyms:Hydrazine,(3,4-xylyl)- (8CI); (3,4-Dimethylphenyl)hydrazine; (3,4-Xylyl)hydrazine

Chemical Property of 3,4-Dimethylphenylhydrazine hydrochloride

Chemical Property:

• Melting Point: 49.5-52℃
• Density: 1.058

Purity/Quality:

98%min ^*data from raw suppliers

(3,4-Dimethylphenyl)hydrazine ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3,4-Dimethylphenylhydrazine hydrochloride

There total 3 articles about 3,4-Dimethylphenylhydrazine hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-amino-o-xylene (95-64-7) → 3,4-dimethylphenylhydrazine (13636-53-8)

Guidance literature:

Diazotization_.man reduziert das Diazoniumsalz zuerst mit Natriumsulfit, dann mit Zink und Essigsaeure;

Reference yield:

3,4-dimethyl-benzenediazonium; chloride (69457-08-5) → 3,4-dimethylphenylhydrazine (13636-53-8)

Guidance literature:

With water; sodium sulfite; at 70 - 75 ℃; for 0.5h;

DOI:10.1134/S1070428017040157

Reference yield:

→ 3,4-dimethylphenylhydrazine (13636-53-8)

Guidance literature:

Natrium-Salz der 3,4-Dimethyl-benzol-sulfonsaeure, Natrium-hydrazid, Hydrazin, Ether, 15grad;

upstream raw materials:

4-amino-o-xylene

3,4-dimethyl-benzenediazonium; chloride

Downstream raw materials:

acetic acid N'-(3,4-dimethylphenyl)hydrazide

2-(3,4-dimethylphenyl)-5-phenyl-2,4-dihydropyrazol-3-one

ethyl 1-(3,4-dimethylphenyl)-5-phenyl-1H-pyrazole-3-carboxylate

2-(3,4-dimethylphenyl)-2H-indazole

Refernces

• 1、 Wang, Xing,Chen, Yong-Fei,Yan, Wei,Cao, Ling-Ling,Ye, Yong-Hao. "Synthesis and biological evaluation of benzimidazole phenylhydrazone derivatives as antifungal agents against phytopathogenic fungi". . . Retrieved 2016/12/03.