5-bromo-2-methoxy-N-methylbenzenesulfonamide

Base Information

• Chemical Name: 5-bromo-2-methoxy-N-methylbenzenesulfonamide
• CAS No.: 871269-17-9
• Molecular Formula: C₈H₁₀BrNO₃S
• Molecular Weight: 280.142
• Hs Code.: 2935009090
• DSSTox Substance ID: DTXSID10429167
• Wikidata: Q82242119
• Mol file: 871269-17-9.mol

Synonyms:5-bromo-2-methoxy-N-methylbenzenesulfonamide;871269-17-9;5-Bromo-2-methoxy-N-methylbenzenesulphonamide;Benzenesulfonamide,5-bromo-2-methoxy-N-methyl-;SCHEMBL15546364;DTXSID10429167;KZNYMPXBNITLOQ-UHFFFAOYSA-N;MFCD06808832;STK983649;AKOS005140889;AM87282;UPCMLD0ENAT5675096:001;BS-25860;CS-0211881;FT-0644974;5-bromo-2-methoxy-N-methyl-benzenesulfonamide;A841980;Z45527748

Chemical Property of 5-bromo-2-methoxy-N-methylbenzenesulfonamide

Chemical Property:

• Vapor Pressure: 0mmHg at 25°C
• Melting Point: 126-128
• Boiling Point: 389.467°C at 760 mmHg
• Flash Point: 189.343°C
• PSA: 63.78000
• Density: 1.554g/cm³
• LogP: 2.83750
• Storage Temp.: Keep Cold
• XLogP3: 1.6
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 3
• Exact Mass: 278.95648
• Heavy Atom Count: 14
• Complexity: 275

Purity/Quality:

98%min ^*data from raw suppliers

5-Bromo-2-methoxy-N-methylbenzenesulfonamide ^*data from reagent suppliers

Safty Information:

• Hazard Codes: Xi

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CNS(=O)(=O)C1=C(C=CC(=C1)Br)OC

Technology Process of 5-bromo-2-methoxy-N-methylbenzenesulfonamide

There total 1 articles about 5-bromo-2-methoxy-N-methylbenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.63%

5-bromo-2-methoxybenzenesulfonyl chloride (23095-05-8) + methylamine hydrochloride (593-51-1) → 5-bromo-2-methoxy-N-methylbenzenesulfonamide (871269-17-9)

Guidance literature:

With triethylamine; In dichloromethane; at 0 - 20 ℃; for 3h; Cooling with ice;

upstream raw materials:

5-bromo-2-methoxybenzenesulfonyl chloride

methylamine hydrochloride

Refernces