Diethyl decylphosphonate

Base Information

• Chemical Name: Diethyl decylphosphonate
• CAS No.: 16165-68-7
• Molecular Formula: C14H31O3P
• Molecular Weight: 278.372
• Hs Code.: 2931900090
• DSSTox Substance ID: DTXSID70378647
• Nikkaji Number: J1.526.377F
• Wikidata: Q82168150
• Mol file: 16165-68-7.mol

Synonyms:16165-68-7;Diethyl 1-decylphosphonate;1-diethoxyphosphoryldecane;diethyl decylphosphonate;Phosphonic acid, P-decyl-, diethyl ester;Decylphosphonic acid diethyl ester;diethyl decanephosphonate;Diethyl n-decanephosphonate;Diethyl(1-decyl)phosphonate;SCHEMBL503511;DTXSID70378647;decyl-phosphonic acid diethyl ester;n-decylphosphonic acid diethyl ester;MFCD00015593;AKOS015839006;Phosphonic acid,p-decyl-,diethyl ester;CS-0447608;FT-0624815

Chemical Property of Diethyl decylphosphonate

Chemical Property:

• Vapor Pressure: 9.59E-05mmHg at 25°C
• Refractive Index: 1.4390
• Boiling Point: 349.3 °C at 760 mmHg
• Flash Point: 178.7 °C
• PSA: 45.34000
• Density: 0.938 g/cm³
• LogP: 5.39320
• XLogP3: 4.7
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 13
• Exact Mass: 278.20108184
• Heavy Atom Count: 18
• Complexity: 209

Purity/Quality:

98% ^*data from raw suppliers

DIETHYL 1-DECYLPHOSPHONATE 95.00% ^*data from reagent suppliers

Safty Information:

• Safety Statements: 24/25

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CCCCCCCCCCP(=O)(OCC)OCC

Technology Process of Diethyl decylphosphonate

There total 6 articles about Diethyl decylphosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

→ diethyl n-decylphosphonate (16165-68-7)

Guidance literature:

Reference yield:

1-bromo dodecane (112-29-8) + triethyl phosphite (122-52-1) → ethyl bromide (74-96-4) + diethyl n-decylphosphonate (16165-68-7)

Guidance literature:

DOI:10.1039/DT9810002423

Reference yield:

1-bromo dodecane (112-29-8) + triethyl phosphite (122-52-1) → diethyl n-decylphosphonate (16165-68-7)

Guidance literature:

at 150 - 160 ℃;

DOI:10.1021/ja01223a046

upstream raw materials:

1-Decene

phosphonic acid diethyl ester

1-bromo dodecane

triethyl phosphite

Downstream raw materials:

1-decylphosphonic acid

Refernces

• 1、 Yang, Bin,Zhang, Hong-Yu,Yang, Shang-Dong. "Copper-catalyzed allylic C-H phosphonation". supporting information. p. 3561 - 3565. Retrieved 2015/03/30.
• 2、 Wozniak, Michel,Nowogrocki, Guy. "Phosphonate Complexes. Part 6. Influence of Steric Effects, Solvation, and Chelation on Stability". . p. 2423 - 2428. Retrieved 2007/10/02.