C₂₉H₂₂N₆S₂

Base Information

• Chemical Name: C₂₉H₂₂N₆S₂
• CAS No.: 1429045-76-0
• Molecular Formula: C₂₉H₂₂N₆S₂
• Molecular Weight: 518.666
• Mol file: 1429045-76-0.mol

Synonyms:C₂₉H₂₂N₆S₂

Chemical Property of C₂₉H₂₂N₆S₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₂₉H₂₂N₆S₂

There total 8 articles about C₂₉H₂₂N₆S₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C48H36N6S2 → C29H22N6S2 (1429045-76-0)

Guidance literature:

With hydrogenchloride; water; In tetrahydrofuran; at 20 ℃; for 16h;

DOI:10.1016/j.bmc.2013.01.067

Reference yield:

tributyl(p-tolyl)stannane (31614-66-1) → C29H22N6S2 (1429045-76-0)

Guidance literature:

Multi-step reaction with 5 steps

1: bis-triphenylphosphine-palladium(II) chloride; lithium chloride / N,N-dimethyl-formamide / Inert atmosphere

2: sodium azide; tributyltin chloride / toluene / Reflux

3: N-Bromosuccinimide; dibenzoyl peroxide / tetrachloromethane

4: potassium carbonate / N,N-dimethyl-formamide / 12 h / 20 °C / Inert atmosphere

5: hydrogenchloride; water / tetrahydrofuran / 16 h / 20 °C

With hydrogenchloride; bis-triphenylphosphine-palladium(II) chloride; N-Bromosuccinimide; sodium azide; tributyltin chloride; water; potassium carbonate; lithium chloride; dibenzoyl peroxide; In tetrahydrofuran; tetrachloromethane; N,N-dimethyl-formamide; toluene;

DOI:10.1016/j.bmc.2013.01.067

Reference yield:

o-cyanobromobenzene (2042-37-7) → C29H22N6S2 (1429045-76-0)

Guidance literature:

Multi-step reaction with 5 steps

1: bis-triphenylphosphine-palladium(II) chloride; lithium chloride / N,N-dimethyl-formamide / Inert atmosphere

2: sodium azide; tributyltin chloride / toluene / Reflux

3: N-Bromosuccinimide; dibenzoyl peroxide / tetrachloromethane

4: potassium carbonate / N,N-dimethyl-formamide / 12 h / 20 °C / Inert atmosphere

5: hydrogenchloride; water / tetrahydrofuran / 16 h / 20 °C

With hydrogenchloride; bis-triphenylphosphine-palladium(II) chloride; N-Bromosuccinimide; sodium azide; tributyltin chloride; water; potassium carbonate; lithium chloride; dibenzoyl peroxide; In tetrahydrofuran; tetrachloromethane; N,N-dimethyl-formamide; toluene;

DOI:10.1016/j.bmc.2013.01.067

upstream raw materials:

tributyl(p-tolyl)stannane

o-cyanobromobenzene

N-triphenylmethyl-5-(4'-methylbiphenyl-2-yl)tetrazole

2-(benzylsulfanyl)quinazolin-4(3H)-one

Refernces