PALLADIUM(II) NITRATE HYDRATE

Base Information

• Chemical Name: PALLADIUM(II) NITRATE HYDRATE
• CAS No.: 82279-70-7
• Molecular Formula: H₄N₂O₈Pd
• Molecular Weight: 266.46
• Hs Code.: 2843900090
• Mol file: 82279-70-7.mol

Synonyms:Palladium nitrate;

Chemical Property of PALLADIUM(II) NITRATE HYDRATE

Chemical Property:

• PSA: 146.99000
• LogP: 0.50390

Purity/Quality:

99% ^*data from raw suppliers

Palladium(II) nitrate hydrate ^*data from reagent suppliers

Safty Information:

• Pictogram(s): O,Xi
• Hazard Codes: O,Xi
• Statements: 8-36/37/38
• Safety Statements: 17-26-36/37/39

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of PALLADIUM(II) NITRATE HYDRATE

There total 1 articles about PALLADIUM(II) NITRATE HYDRATE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

water (7732-18-5) + nitric acid (7697-37-2,78989-43-2) + palladium (7440-05-3) → trans-dinitratodiaquapalladium(II) (82279-70-7,1147543-08-5)

Guidance literature:

With HCl; In nitric acid; aq. HNO3; Pd powder dissolved at 90-95°C within 1 h in HNO3 (d. 1.419 g/ml)with addn. of HCl (d. 1.165 g/ml), then soln. evapd. at the same temp., diluted with water; concd. in air to wet crystals, dried in desiccator for 1-2 d over KOH; elem. anal.;

DOI:10.1134/S1070427207050023

Reference yield: 85.0%

trans-dinitratodiaquapalladium(II) (82279-70-7,1147543-08-5) + acetic acid (64-19-7,77671-22-8) → palladium diacetate (3375-31-3)

Guidance literature:

In acetic acid; Pd(II) nitrate dissolved in anhyd. acetic acid; stirred for 3 h at room temp.; suspn. diluted with acetic acid; centrifuged; washed (H2O, acetone); dried (vac., NaOH); elem. anal.;

DOI:10.1134/S003602361110024X

Reference yield: 61.0%

trans-dinitratodiaquapalladium(II) (82279-70-7,1147543-08-5) + acetic acid (64-19-7,77671-22-8) → palladium (II) acetate + palladium diacetate (3375-31-3)

Guidance literature:

In water; acetic acid; Pd(II) nitrate dissolved in mixt. of acetic acid and H2O; mixt. stirred for 3 h at room temp.; filtered; washed (glacial acetic acid, ether); dried (vac. over alkali);mixt. extd. (benzene); filtered; filtrate evapd. to dryness at 40.degre e.C in vac.; elem. anal.;

DOI:10.1134/S003602361110024X

upstream raw materials:

water

nitric acid

palladium

Downstream raw materials:

palladium diacetate

Refernces