triphenylantimony o-hydroxy-o-phenylenediamine

Base Information Edit

Chemical Name:triphenylantimony o-hydroxy-o-phenylenediamine
CAS No.:187221-61-0
Molecular Formula:C₂₄H₁₉O₃Sb
Molecular Weight:477.163
Hs Code.:
Mol file:187221-61-0.mol

Synonyms:triphenylantimony o-hydroxy-o-phenylenediamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of triphenylantimony o-hydroxy-o-phenylenediamine Edit

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Technology Process of triphenylantimony o-hydroxy-o-phenylenediamine

There total 1 articles about triphenylantimony o-hydroxy-o-phenylenediamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 603-36-1
triphenylantimony

: 87-66-1
2-hydroxyresorcinol

: 187221-61-0
triphenylantimony o-hydroxy-o-phenylenediamine

Guidance literature:: With tert.-butylhydroperoxide; sodium sulfate; In tetrahydrofuran; byproducts: tert-butyl alcohol; anaerobic conditions, polyphenol, peroxide, sodium sulfate, and solvent addn. into one knee of H-shaped ampule, soln. of Sb-compd. addn. to the other knee, repeated degassing, slow mixing with cooling (1 h, 0°C), shaking, stirring (1 h); volatiles condensation in trap, slid residue sepn. from Na2SO4, recrystn. (THF-hexane, anaerobic conditions); elem. anal.;