OLEIC ACID (9,10-D2)

Base Information

• Chemical Name: OLEIC ACID (9,10-D2)
• CAS No.: 5711-29-5
• Molecular Formula: C18H32 D2 O2
• Molecular Weight: 284.451
• Mol file: 5711-29-5.mol

Synonyms:(Z)-9-Octadecenoic-9,10-d2acid; cis-9-Octadecenoic-9,10-d2 acid

Chemical Property of OLEIC ACID (9,10-D2)

Chemical Property:

• Melting Point: 13.4 °C(lit.)
• Boiling Point: 192-195 °C/1.2 mmHg(lit.)
• PSA: 37.30000
• Density: 0.896 g/mL at 25 °C
• LogP: 6.10850
• Storage Temp.: -20°C

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of OLEIC ACID (9,10-D2)

There total 3 articles about OLEIC ACID (9,10-D2) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

Stearolic acid (506-24-1) → <9,10-2H2>-oleic acid (5711-29-5)

Guidance literature:

With quinoline; deuterium; Pd-BaSO₄; In hexane;

DOI:10.1021/jf950570w

Reference yield:

methyl <9,10-(2)H2>octadec-9Z-enoate (35356-36-6) → <9,10-2H2>-oleic acid (5711-29-5)

Guidance literature:

With potassium hydroxide;

DOI:10.1021/ja01132a019

Reference yield:

stearolic acid methyl ester (1120-32-7) → <9,10-2H2>-oleic acid (5711-29-5)

Guidance literature:

Multi-step reaction with 2 steps

1: Raney nickel; dioxane; deuterium

2: ethanolic KOH-solution

With 1,4-dioxane; potassium hydroxide; nickel; deuterium;

DOI:10.1021/ja01132a019

upstream raw materials:

methyl <9,10-(2)H2>octadec-9Z-enoate

Stearolic acid

stearolic acid methyl ester

Downstream raw materials:

2(3H)-furanone, dihydro-5-(2-octenyl)-, (Z)-

(R)-5-Hexyl-dihydro-furan-2-one

Refernces

• 1、 Valiente, Alejandro,Martínez-Pardo, Pablo,Kaur, Gurpreet,Johansson, Magnus J.,Martín-Matute, Belén. "Electrochemical Proton Reduction over Nickel Foam for Z-Stereoselective Semihydrogenation/deuteration of Functionalized Alkynes". . . Retrieved 2021/12/22.