Butanamide, 2-[(4-chloro-2-nitrophenyl)azo]-N-(2-chlorophenyl)-3-oxo-

Base Information

• Chemical Name: Butanamide, 2-[(4-chloro-2-nitrophenyl)azo]-N-(2-chlorophenyl)-3-oxo-
• CAS No.: 6486-23-3
• Deprecated CAS: 10347-17-8,11129-86-5,50642-22-3,477904-36-2
• Molecular Formula: C16H12Cl2N4O4
• Molecular Weight: 395.202
• Hs Code.: 2927000090
• European Community (EC) Number: 229-355-1
• NSC Number: 17264
• UNII: L885GOC9B6
• DSSTox Substance ID: DTXSID40863873
• Nikkaji Number: J34.095B
• Wikidata: Q27282827
• Mol file: 6486-23-3.mol

Synonyms:6486-23-3;Carnelio Yellow 10G;Eljon Fast Yellow 10G;Fast Yellow 10J;Fast Yellow 15J;Irgalite Yellow VG;Monolite Fast Yellow 10G;Toluidine Yellow AH 177;Fast Yellow 10JT;Irgalite Yellow VGT;Irgalite Yellow VGX;Siegle Yellow 10G;Versal Yellow 10G;Vulcol Yellow 10G;Permanent Yellow Toner 10G;Fastona Yellow 10G;Hansa Yellow 10GD;Hansa Yellow 10GT;Irgalite Yellow PV4;Oralith Yellow 10G;Silopol Yellow 10G;Hostaperm Yellow IOG;Hansa Yellow 10-G;Irgalite Yellow 10G;Monolite Yellow 10G;Permansa Yellow 10G;Silosol Yellow 10GN;Arylamide Yellow 10G;Chromatex Yellow 10J;Graphtol Yellow 10GL;Hancock Yellow 1007;Siloton Yellow 10GCL;Helio Fast Yellow 8GM;Isol Aryl Yellow 10G;Mono Fast Yellow 10G;Sanyo Fast Yellow 10G;Syton Fast Yellow 10G;Hansa Yellow 10G extra;Isol Aryl Yellow 10GX;Hansa Yellow 10G Toner;Eljon Fast Yellow 10GX;Kromon Yellow 10G Extra;Lutetia Fast Yellow 10J;Lutetia Fast Yellow 12J;Dainichi Fast Yellow 10G;Iroquois Yellow X-1285;Recolite Fast Yellow 10G;Segnale Light Yellow 10G;Symuler Fast Yellow 10GH;Irgalite Fast Yellow P10G;Monolite Fast Yellow 10GA;Monolite Fast Yellow 10GV;Recolite Fast Yellow 10GT;Monolite Fast Yellow 10GBA;Eljon Fast Primrose PV Extra;Hansa Yellow 10G;Fanchon Yellow (10G) YH-4;Monolite Fast Paper Yellow 10G;Permanent Yellow 10G YT-372;C.I. 11710;Phthalocyanine Light Fast Yellow 2Z;2-[(4-Chloro-2-nitrophenyl)azo]-N-(2-chlorophenyl)-3-oxobutyramide;UNII-L885GOC9B6;Butanamide, 2-[(4-chloro-2-nitrophenyl)azo]-N-(2-chlorophenyl)-3-oxo-;CI 11710;L885GOC9B6;2-[(4-chloro-2-nitrophenyl)diazenyl]-N-(2-chlorophenyl)-3-oxobutanamide;EINECS 229-355-1;NSC 17264;NSC-17264;Butanamide, 2-((4-chloro-2-nitrophenyl)azo)-N-(2-chlorophenyl)-3-oxo-;EC 229-355-1;2-((4-Chloro-2-nitrophenyl)azo)-N-(2-chlorophenyl)-3-oxobutyramide;Butanamide, 2-(2-(4-chloro-2-nitrophenyl)diazenyl)-N-(2-chlorophenyl)-3-oxo-;Butanamide, 2-[2-(4-chloro-2-nitrophenyl)diazenyl]-N-(2-chlorophenyl)-3-oxo-;SCHEMBL340984;JAUNE COVANOR W 1603;SCHEMBL12760919;SCHEMBL12760920;DTXSID40863873;CI 11710 [INCI];NSC17264;MFCD00071936;AKOS025310987;AKOS037643361;Butanamide, 2-[(4-chloro-2-nitrophenyl) azo]-N-(2-chlorophenyl)-3-oxo-;AS-15319;C.I.11710;A923734;Q27282827;ACETOACETANILIDE, 2'-CHLORO-2-(4-CHLORO-2-NITROPHENYLAZO)-;.ALPHA.-(4-CHLORO-2-NITROPHENYLAZO)ACETOACETIC ACID O-CHLOROANILIDE;2-((4-Chloro-2-nitrophenyl)azo)-N-(2-chlorophenyl)-3-oxobutanamid- e;2-((4-Chloro-2-nitrophenyl)azo)-N-(2-chlorophpenyl)-3-oxobutanami- de;2-(4-Chloro-2-nitro-phenylazo)-N-(2-chloro-phenyl)-3-oxo-butyramide;Crotonanilide, 2'-chloro-2-[(4-chloro-2-nitrophenyl)azo]-3-hydroxy-;2- [(4- chloro- 2- nitrophenyl)azo]- N- (2- chlorophenyl)- 3- oxobutyramide;2-Butenamide, 2-[(4-chloro-2-nitrophenyl)azo]-N-(2-chlorophenyl)-3-hydroxy-

Chemical Property of Butanamide, 2-[(4-chloro-2-nitrophenyl)azo]-N-(2-chlorophenyl)-3-oxo-

Chemical Property:

• Appearance/Colour: light yellow powder
• Vapor Pressure: 1.56E-12mmHg at 25°C
• Melting Point: 256 - 258ºC
• Refractive Index: 1.65
• Boiling Point: 559.1 °C at 760 mmHg
• PKA: 6.83±0.59(Predicted)
• Flash Point: 291.9 °C
• PSA: 116.71000
• Density: 1.49 g/cm³
• LogP: 5.17780
• XLogP3: 4.6
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 6
• Rotatable Bond Count: 5
• Exact Mass: 394.0235603
• Heavy Atom Count: 26
• Complexity: 569

Purity/Quality:

99% ^*data from raw suppliers

Pigment Yellow 3 ^*data from reagent suppliers

Safty Information:

• Pictogram(s): E,C,N
• Hazard Codes: E,C,N

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC(=O)C(C(=O)NC1=CC=CC=C1Cl)N=NC2=C(C=C(C=C2)Cl)[N+](=O)[O-]

Technology Process of Butanamide, 2-[(4-chloro-2-nitrophenyl)azo]-N-(2-chlorophenyl)-3-oxo-

There total 3 articles about Butanamide, 2-[(4-chloro-2-nitrophenyl)azo]-N-(2-chlorophenyl)-3-oxo- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-oxo-N-2-chlorophenylbutanamide (93-70-9) + 4-Chloro-2-nitroaniline (89-63-4) → lemon yellow 651 (6486-23-3)

Guidance literature:

4-Chloro-2-nitroaniline; With hydrogenchloride; C₂₆H₂₈N₆O₄S; In water; at 10 ℃; for 1h;

3-oxo-N-2-chlorophenylbutanamide; With sodium hydroxide; acetic acid; In water; at 25 - 90 ℃; for 2.5h; pH=6;

Reference yield:

4-Chloro-2-nitroaniline (89-63-4) → lemon yellow 651 (6486-23-3)

Guidance literature:

Multi-step reaction with 2 steps

1: HCl, sodium nitrite / H₂O / 0 °C

2: 10percent NaOH / aq. ethanol

With hydrogenchloride; sodium hydroxide; sodium nitrite; In ethanol; water;

Reference yield:

3-oxo-N-2-chlorophenylbutanamide (93-70-9) + 4-chloro-2-nitro-benzenediazonium; chloride (119-09-5) → lemon yellow 651 (6486-23-3)

Guidance literature:

With sodium hydroxide; In ethanol; Yield given;

upstream raw materials:

3-oxo-N-2-chlorophenylbutanamide

4-chloro-2-nitro-benzenediazonium; chloride

4-Chloro-2-nitroaniline

Refernces

• 1、 Jain,Dixit,Pandey. "Synthesis of some new 1-carbamoyl-3-aminophenyl- and 1-carbamoyl-3-amino-(2-chlorophenyl)-5-methyl-4-arylazopyrazoles as possible potential antidiabetics". . p. 486 - 489. Retrieved 2007/10/02.