1-(4-Bromophenyl)octane

Base Information

• Chemical Name: 1-(4-Bromophenyl)octane
• CAS No.: 51554-93-9
• Molecular Formula: C14H21 Br
• Molecular Weight: 269.225
• Hs Code.: 2903999090
• Mol file: 51554-93-9.mol

Synonyms:Octane,1-(p-bromophenyl)- (4CI); 1-(4-Bromophenyl)octane; 1-Bromo-4-n-octylbenzene;1-Bromo-4-octylbenzene; 4-Octyl-1-bromobenzene; 4-Octylbromobenzene;4-n-Octylbromobenzene; p-Octylbromobenzene

Chemical Property of 1-(4-Bromophenyl)octane

Chemical Property:

• Appearance/Colour: Colorless liquid
• Vapor Pressure: 0.000897mmHg at 25°C
• Refractive Index: 1.5130-1.5160
• Boiling Point: 199-201 ºC
• Flash Point: 176.5 °C
• PSA: 0.00000
• Density: 1.13 g/cm³
• LogP: 5.35210
• Storage Temp.: Sealed in dry,Room Temperature

Purity/Quality:

1-Bromo-4-N-octylbenzene ^*data from reagent suppliers

Safty Information:

• Safety Statements: 24/25

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-(4-Bromophenyl)octane

There total 13 articles about 1-(4-Bromophenyl)octane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

1-octyl-4-(trimethylsilyl)benzene → 1-bromo-4-octylbenzene (51554-93-9)

Guidance literature:

With bromine; In dichloromethane; at -78 ℃; for 0.133333h;

Reference yield: 87.0%

1.4-dibromobenzene (106-37-6) + octylmagnesium bromide (17049-49-9) → 1-bromo-4-octylbenzene (51554-93-9)

Guidance literature:

With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In diethyl ether; at 20 ℃; for 1h;

Reference yield: 86.0%

1-(4-bromo-phenyl)-oct-1-ene (76287-60-0) → 1-bromo-4-octylbenzene (51554-93-9)

Guidance literature:

With hydrogen; platinum(IV) oxide; In ethanol;

upstream raw materials:

1-(4-bromo-phenyl)-octan-1-ol

1-(4-bromo-phenyl)-oct-1-ene

1.4-dibromobenzene

octylmagnesium bromide

Downstream raw materials:

1-(6-Bromo-hexyl)-4-octyl-benzene

bis(4-octylphenyl)-(4'-trimethylsilylbiphenyl-2-yl)methanol

(4-octylphenyl)boronic acid

Refernces

• 1、 Tang, Ren-Jin,Milcent, Thierry,Crousse, Benoit. "Regioselective Halogenation of Arenes and Heterocycles in Hexafluoroisopropanol". . p. 930 - 938. Retrieved 2018/01/28.
• 2、 -. "Synthesis method of p-bromo-linear alkylbenzene". Paragraph 0035; 0055. . Retrieved 2017/08/25.