4-(1,4-Dioxaspiro[4.5]decan-8-yl)cyclohexanone

Base Information Edit

Chemical Name:4-(1,4-Dioxaspiro[4.5]decan-8-yl)cyclohexanone
CAS No.:56309-94-5
Molecular Formula:C14H22O3
Molecular Weight:238.327
Hs Code.:2932999099
European Community (EC) Number:423-860-2,611-378-7
DSSTox Substance ID:DTXSID10355639
Nikkaji Number:J1.641.687H
Wikidata:Q72486949
Mol file:56309-94-5.mol

Synonyms:56309-94-5;Ketoketal;4-(1,4-Dioxaspiro[4.5]decan-8-yl)cyclohexanone;4-(1,4-dioxaspiro[4.5]decan-8-yl)cyclohexan-1-one;8-(4-Oxocyclohexyl)-1,4-dioxaspiro[4.5]decane;Bicyclohexane-4,4-dione Monoethylene Ketal;4-(1,4-dioxaspiro[4.5]dec-8-yl)cyclohexanone;1,1'-Bicyclohexane-4,4'dione monoethylene ketal;Cyclohexanone, 4-(1,4-dioxaspiro[4.5]dec-8-yl)-;Bicyclohexane-4,4'-dione Monoethylene Ketal;C14H22O3;MFCD00809704;4,4 inverted exclamation mark -Dicyclohexanedione monoethylene ketal;EC 423-860-2;4-(1,4-dioxa-spiro(4.5)dec-8-yl)-cyclohexanone;Cyclohexanone, 4-(1,4-dioxaspiro(4.5)dec-8-yl)-;BAS 00451572;4-{1,4-DIOXASPIRO[4.5]DECAN-8-YL}CYCLOHEXAN-1-ONE;Dicyclohexane-4,4'-dione monoethylene ketal;Oprea1_121109;Oprea1_868255;SCHEMBL422994;AMY8749;DTXSID10355639;HMS1672N02;AKOS000618687;CS-W014148;Bicyclohexane-4,4-dioneMonoethyleneKetal;AC-26253;AS-67312;SY029814;4,4'-Dicyclohexanedione monoethylene ketal;bicyclohexane-4,4'-dione monoethyleneacetal;B3405;FT-0652524;Ketoketal(bicyclohexane-4,4 -dione monoethyl);A24046;D70956;4-(1,4-dioxaspiro[4,5]dec-8-yl)cyclohexanone;4-(1,4-Dioxa-spiro[4.5]dec-8-yl)cyclohexanone;4-(1,4-dioxaspiro[4,5]dec-8-yl)-cyclohexanone;8-(4-oxocyclohexyl)-1,4-dioxaspiro[4,5]decane;4-(1,4-dioxaspiro[4,5]decane-8-yl)cyclohexanone;4-(1,4-dioxaspiro[4.5]decan-8-yl)-cyclohexanone;J-521620;Dicyclohexane-4,4 inverted exclamation mark -dione monoethylene ketal

Suppliers and Price of 4-(1,4-Dioxaspiro[4.5]decan-8-yl)cyclohexanone

Supply Marketing:Edit

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
Ketoketal
500mg
$ 75.00

TRC
Ketoketal
100mg
$ 60.00

TCI Chemical
Bicyclohexane-4,4'-dione Monoethylene Ketal >98.0%(GC)
25g
$ 118.00

TCI Chemical
Bicyclohexane-4,4'-dione Monoethylene Ketal >98.0%(GC)
5g
$ 40.00

Matrix Scientific
4-(1,4-Dioxaspiro[4.5]decan-8-yl)cyclohexanone 97%
1g
$ 38.00

Matrix Scientific
4-(1,4-Dioxaspiro[4.5]decan-8-yl)cyclohexanone 97%
5g
$ 101.00

Matrix Scientific
4-(1,4-Dioxaspiro[4.5]decan-8-yl)cyclohexanone 97%
10g
$ 158.00

Crysdot
4-(1,4-Dioxaspiro[4.5]decan-8-yl)cyclohexanone 97%
500g
$ 458.00

Chemenu
4-(1,4-Dioxaspiro[4.5]decan-8-yl)cyclohexanone 97%
500g
$ 428.00

American Custom Chemicals Corporation
KETOKETAL 95.00%
50G
$ 2562.42

Total 104 raw suppliers

Chemical Property of 4-(1,4-Dioxaspiro[4.5]decan-8-yl)cyclohexanone Edit

Chemical Property:

Appearance/Colour:White crystal
Vapor Pressure:0.064Pa at 20℃
Melting Point:100.0 to 104.0 °C
Boiling Point:365.4 °C at 760 mmHg
Flash Point:166.2 °C
PSA：35.53000
Density:1.11 g/cm³
LogP:2.67900
Storage Temp.:Sealed in dry,Room Temperature
Water Solubility.:Insoluble in water.
XLogP3:1.6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:1
Exact Mass:238.15689456
Heavy Atom Count:17
Complexity:274

Purity/Quality:

99% ^*data from raw suppliers

Ketoketal ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1CC(=O)CCC1C2CCC3(CC2)OCCO3
Uses Ketoketal is used as a pharmaceutical intermediate. Intermediates of Liquid Crystals

Technology Process of 4-(1,4-Dioxaspiro[4.5]decan-8-yl)cyclohexanone

There total 2 articles about 4-(1,4-Dioxaspiro[4.5]decan-8-yl)cyclohexanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.6%

: 23391-99-3
4,4'-bicyclohexanone

: 107-21-1
ethylene glycol

: 56309-94-5
8-(4-oxocyclohexyl)-1,4-dioxaspiro[4.5]decane

Guidance literature:: 4,4'-bicyclohexanone; phosphoric acid; In water; pentane; at 37 ℃; for 1h; Heating / reflux;

ethylene glycol; In pentane; at 26 - 37 ℃; for 5.5 - 21.9h; Product distribution / selectivity; Heating / reflux;